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US 5,292,585 AGranted
Magnetic recording medium comprising a magnetic film layer and a coating of purified perfluoropolyther lubricant
AssigneeTosoh Corporation
InventorsYukio Ohnuki, Satoshi Kurosawa, Akio Kondo
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Abstract
A magnetic recording medium having coated thereon a lubricant of such a purity that no impurities and low molecular weight species are substantially detected by gel permeation chromatography.
Claims4
A magnetic recording medium comprising a magnetic film layer having coated thereon a layer of purified perfluoropolyether lubricant having the formula:
- Piperonyl--OCH.sub.2 CF.sub.2 O--(CF.sub.2 CF.sub.2 O).sub.n --(CF.sub.2 O).sub.m --CF.sub.2 CH.sub.2 O--Piperonyl
- which lubricant has a weight-average molecular weight of at least 2000 and a weight-average molecular weight/number average molecular weight ratio of not more than 1.3 and which contains no chemical species having a molecular weight of less than about 700, and wherein said lubricant has been purified by
- 1) dissolving said lubricant in a good solvent to obtain a uniform solution,
- 2) adding to the solution of lubricant in good solvent a poor solvent under stirring in an amount of from 4-5 times the amount of good solvent already present,
- 3) thoroughly mixing the solution obtained in (2),
- 4) allowing the mixed solution obtained in (3) to stand still and phase separate,
- 5) collecting the good solvent containing the lubricant,
- 6) repeating steps (2)-(4) at least three times,
- 7) removing the good solvent from the lubricant,
- 8) filtering the lubricant.
7 more elements
Dependencies are inferred from the claim text.