Process and apparatus for air fractionation by rectification
AssigneeLinde Aktiengesellschaft
InventorDietrich Rottmann
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Abstract
For air fractionation by two-stage rectification with subsequent production of crude argon, a component stream of the crude argon stream (25, 31) withdrawn from the crude argon column (2) is condensed (35) in indirect heat exchange (34) with a liquid oxygen product stream (40) from the medium pressure column (4), the oxygen product stream (40) being partially vaporized. The condensed crude argon (35) is then recycled into the crude argon column (20). A second component stream of the crude argon is obtained as the product (24).
Claims18
In an air fractionation process by rectification, wherein air (1) is compressed, purified, cooled (36), and preliminarily fractionated in a high pressure column (3) of a two-stage rectification column (2) into an oxygen-rich liquid (6) and into a nitrogen-rich fraction (5), the oxygen-rich liquid (6) and/or nitrogen-rich fraction (5) being fed at least in part to the medium pressure column (4) of the rectification column (2) and separated into oxygen and nitrogen, and wherein an argon-containing oxygen stream (17) and an oxygen product stream (40) are withdrawn from the medium pressure column (4), the argon-containing oxygen stream being introduced into a crude argon column (20) operated under a pressure lower than the pressure of the medium pressure column (4), and gaseous crude argon (21) being removed from an upper zone of said crude argon column, the improvement wherein the oxygen product stream (40) is discharged in the liquid condition from the medium pressure column (4), at least a portion (31) of the gaseous crude argon withdrawn from the crude argon column (20) is condensed in indirect heat exchange (34) against the liquid oxygen product stream (40), the oxygen product stream (40) being at least partially vaporized, and resultant condensed crude argon (35) is reintroduced into the crude argon column (20).
Dependencies are inferred from the claim text.