Method for preparing a fused silica glass body co-doped with a rare earth element and aluminum
AssigneesShin-Etsu Chemical Co., Ltd., Kokusai Denshin Denwa Kabushiki Kaisha
InventorsNoboru Edagawa, Yoshihiro Yoshida, Minoru Taya, Tadakatsi Shimada, Kazuo Koya
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Abstract
A novel method is proposed for the preparation of a transparent fused silica glass body co-doped with a rare earth element and aluminum each in a high uniformity of the dopant distribution. The method comprises the steps of: (a) flame-hydrolyzing a silicon compound and an aluminum compound in an oxyhydrogen flame to form a porous silicon oxide body containing aluminum; (b) soaking the porous body having a specified bulk density with a solution of a rare earth compound; (c) drying the solution-soaked porous body; and (d) sintering and vitrifying the dried porous body into a transparent glass body.
Claims7
A method for the preparation of a fused silica glass body co-doped with a rare earth element and aluminum which comprises the successive steps of:
- (a) introducing a silicon compound in the form of vapor and an aluminum compound in the form of vapor into an oxyhydrogen flame to effect co-pyrolysis of the silicon and aluminum compounds into their respective oxides in the form of particles which are deposited on a substrate in the form of a porous silicon oxide body containing aluminum oxide;
- (b) soaking the porous body of silicon oxide containing aluminum oxide with a solution of a compound of a rare earth element in a solvent to impregnate the porous body;
- (c) drying the porous body of silicon oxide impregnated with the solution;
- and
- (d) heating the dried porous body of silicon oxide containing aluminum oxide and the rare earth compound at an elevated temperature to effect sintering and vitrification thereof into a transparent fused silica glass body co-doped with the rare earth element and aluminum.
Dependencies are inferred from the claim text.