# US 5,241,369 A · Two-dimensional optical scatterometer apparatus and process

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- Number: US 5,241,369 A
- Document ID: US5241369A
- Status: Granted
- Kind: A
- Application number: 07/591,452
- Filed: 1990-10-01
- Granted: 1993-08-31
- Earliest claimed: 1990-10-01
- Inventors: John R. McNeil; Scott R. Wilson
- Web page: https://patentgrep.com/patent/US5241369A

## CPC

- G01B 11/303: {using photoelectric detection means}
- G01N 21/474: {Details of optical heads therefor, e.g. using optical fibres}
- G01N 21/49: within a body or fluid
- G01N 21/55: Specular reflectivity
- G01N 21/95: characterised by the material or shape of the object to be examined (G01N21/89 - G01N21/91, G01N21/94 take precedence)
- G01N 2021/4769: {Fluid samples, e.g. slurries, granulates; Compressible powdery of fibrous samples}
- G01B: MEASURING LENGTH, THICKNESS OR SIMILAR LINEAR DIMENSIONS; MEASURING ANGLES; MEASURING AREAS; MEASURING IRREGULARITIES OF SURFACES OR CONTOURS
- G01N: INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES (measuring or testing apparatus or processes other than immunoassay, involving enzymes or microorganisms C12M, C12Q)

## Abstract

An optical scatterometer system includes a screen positioned to receive and display a pattern representative of light specularly reflected and scattered from an illuminated sample material and a camera positioned to record the pattern displayed on the screen. The screen may present a curved surface to increase its light gathering capabilities and may be constructed of an electron trapping material, a photochromic material or a pyrochromic material. The screen may contain one or more apertures for passing one or more incident light beams generated by a light source and/or light specularly reflected and scattered from the sample material. The screen may be positioned between the sample material and the light source, or the sample material may be positioned between the screen and the light source.

## Claims

### Claim 1

An optical scatterometer system comprising:
a sample material having periodic and diffractive microstructure characteristics to be analyzed;
light source means for transmitting an incident light beam to illuminate a point on the sample material;
screen means positioned to receive and display a pattern representative of light specularly reflected from said sample material and light scattered from said sample material, said screen means including one or more apertures for passing said incident light beam and a selected one or both of said light specularly reflected from said sample material and a portion of said light scattered from said sample material, to thereby prevent the selected one or both of said light specularly reflected from said sample material and said portion of said light scattered from said sample material from being received and displayed on said screen means;
camera means positioned to record the pattern displayed on said screen means; and
microprocessor means coupled to said camera means for processing electrical signals received therefrom to provide a two-dimensional intensity distribution of the pattern recorded by said camera means, said two-dimensional intensity distribution being indicative of the periodic and diffractive microstructure characteristics of said sample material.

### Claim 2 (depends on 1)

An optical scatterometer system is in claim 1 wherein said screen means is shaped to form a curved surface to increase its light gathering capabilities and to thereby increase a bandwidth characteristic of the optical scatterometer system.

### Claim 3 (depends on 1)

An optical scatterometer system as in claim 1 wherein said screen means is shaped to form a portion of a sphere.

### Claim 4 (depends on 1)

An optical scatterometer system as in claim 1 wherein said screen means is positioned between said sample material and said light source means.

### Claim 5 (depends on 1)

An optical scatterometer system as in claim 1 wherein said sample material is positioned between said screen means and said light source means.

### Claim 6 (depends on 1)

An optical scatterometer system as in claim 1 wherein said screen means comprises a material having approximately Lambertian optical scattering properties.

### Claim 7 (depends on 1)

An optical scatterometer system as in claim 1 wherein said screen means comprises a material that fluoresces at a wavelength of said incident light beam.

### Claim 8 (depends on 1)

An optical scatterometer system as in claim 1 wherein said screen means comprises an electron trapping material.

### Claim 9 (depends on 1)

An optical scatterometer system as in claim 1 wherein said screen means comprises a photochromic material.

### Claim 10 (depends on 1)

An optical scatterometer system as in claim 1 wherein said screen means comprises a pyrochromic material.

### Claim 11 (depends on 1)

An optical scatterometer system as in claim 1 further comprising removable aperture cover means for covering a selected portion of each of said one or more apertures.

### Claim 12 (depends on 1)

An optical scatterometer system as in claim 1 wherein said one or more apertures are positioned at one or more selected corresponding angles of incidence with respect to an axis of said screen means.

### Claim 13 (depends on 1)

An optical scatterometer system as in claim 1 wherein said incident light beam is transmitted at one or more selected angles of incidence with respect to an axis of said screen means.

### Claim 14 (depends on 1)

An optical scatterometer system as in claim 1 wherein:
said incident light beam is transmitted at one or more selected angles of incidence with respect to an axis of said screen means; and
said incident light beam is transmitted at one or more selected wavelengths.

### Claim 15 (depends on 1)

An optical scatterometer system as in claim 1 wherein:
said incident light beam is transmitted simultaneously at a plurality of selected angles of incidence with respect to an axis of said screen means; and
said incident light beam is transmitted simultaneously at a plurality of selected wavelengths.

### Claim 16 (depends on 1)

An optical scatterometer system as in claim 1 wherein:
said incident light beam is transmitted sequentially at a plurality of selected angles of incidence with respect to an axis of said screen means; and
said incident light beam is transmitted sequentially at a plurality of selected wavelengths.

### Claim 17 (depends on 1)

An optical scatterometer system as in claim 1 wherein said light source means comprises a laser.

### Claim 18 (depends on 1)

An optical scatterometer system as in claim 1 wherein:
said screen means is positioned between said sample material and said light source means;
said screen means is constructed of a material that permits the pattern displayed thereon to be viewed from a side of the screen opposite said sample material; and
said camera means is positioned on a side of said screen means opposite said sample material.

### Claim 19 (depends on 1)

An optical scatterometer system as in claim 1 wherein said camera means and said sample material are both positioned on one side of said screen means.

### Claim 20

An optical scatterometer system comprising:
a sample material having periodic and diffractive microstructure characteristics to be analyzed;
light source means for transmitting an incident light beam to illuminate a point on the sample material;
screen means positioned between said sample material and said light source means to receive and scatter a pattern representative of light specularly reflected from said sample material and light scattered from said sample material, said screen means including an aperture therein through which said incident light beam is directed to illuminate said point on said sample material;
camera means positioned on the same side of said screen means as said light source means;
specularly reflecting curved element positioned on the same side of said screen means as said sample material for directing light scattered from said screen means through said aperture to said camera means for recording thereby; and
microprocessor means coupled to said camera means for processing electrical signals received therefrom to provide a two-dimensional intensity distribution of the light scattered from said screen means and directed through said aperture by said specularly reflecting curved element that is recorded by said camera means, said two-dimensional intensity distribution being indicative of the periodic and diffractive microstructure characteristics of said sample material.

### Claim 21

An optical scatterometer system comprising:
a sample material having periodic and diffractive microstructure characteristics to be analyzed;
light source means for transmitting an incident light beam to illuminate a point on the sample material;
reflector means positioned for receiving said incident light beam and for directing it onto said sample material to illuminate said point on said sample material and for receiving light specularly reflected from said sample material and for directing said light specularly reflected from said sample material away from said optical scatterometer system;
screen means positioned to receive and display a pattern representative of light scattered from said sample material;
camera means positioned to record the pattern displayed on said screen means; and
microprocessor means coupled to said camera means for processing electrical signals received therefrom to provide a two-dimensional intensity distribution of the pattern recorded by said camera means, said two-dimensional intensity distribution being indicative of the periodic and diffractive microstructure characteristics of said sample material.

### Claim 22 (depends on 21)

An optical scatterometer system as in claim 21 wherein said reflector means comprises a mirror.

### Claim 23 (depends on 21)

An optical scatterometer system as in claim 21 wherein said reflector means comprises an optical fiber.

### Claim 24

An optical scatterometer system comprising:
a sample material having periodic and diffractive microstructure characteristics to be analyzed;
light source means for transmitting an incident light beam to illuminate a point on the sample material;
reflector means positioned for receiving said incident light beam and for directing it onto said sample material to illuminate said point on said sample material;
additional reflector means for receiving light specularly reflected from said sample material and for directing said light specularly reflected from said sample material away from said optical scatterometer system;
screen means positioned to receive and display a pattern representative of light scattered from said sample material;
camera means positioned to record the pattern displayed on said screen means; and
microprocessor means coupled to said camera means for processing electrical signals received therefrom to provide a two-dimensional intensity distribution of the pattern recorded by said camera means, said two-dimensional intensity distribution being indicative of the periodic and diffractive microstructure characteristics of said sample material.

### Claim 25 (depends on 24)

An optical scatterometer system as in claim 24 wherein said additional reflector means comprises a beam dump.

### Claim 26

An optical scatterometry process for analyzing periodic and diffractive microstructure characteristics of a sample material, the process comprising the steps of:
transmitting an incident light beam to illuminate a point on the sample material;
positioning a screen to receive and display a pattern representative of light specularly reflected from the sample material and light scattered from the sample material, the screen including one or more apertures therein for passing the incident light beam and a selected one or both of the light specularly reflected from the sample material and a portion of the light scattered from the sample material, to thereby prevent the selected one or both of the light specularly reflected from the sample material and said portion of the light scattered from the sample material from being received and displayed on the screen;
recording the pattern displayed on the screen; and
processing information representative of the pattern recorded to provide a two-dimensional intensity distribution of the pattern recorded, the two-dimensional intensity distribution being indicative of the periodic and diffractive microstructure characteristics of the sample material.

### Claim 27 (depends on 26)

An optical scatterometry process as in claim 26 wherein the incident light beam is transmitted at one or more selected angles of incidence with respect to an axis of the screen.

### Claim 28 (depends on 26)

An optical scatterometry process as in claim 26 wherein:
the incident light beam is transmitted simultaneously at a plurality of selected angles of incidence with respect to an axis of the screen; and
the incident light beam is transmitted simultaneously at a plurality of selected wavelengths.

### Claim 29 (depends on 26)

An optical scatterometry process as in claim 26 wherein:
the incident light beam is transmitted sequentially at a plurality of selected angles of incidence with respect to an axis of the screen; and
the incident light beam is transmitted sequentially at a plurality of selected wavelengths.

### Claim 30

An optical scatterometer system comprising:
a sample material having periodic and diffractive microstructure characteristics to be analyzed;
light source means for transmitting an incident light beam to illuminate a point on the sample material;
screen means positioned between said sample material and said light source means to receive and display a pattern representative of light specularly reflected from said sample material and light scattered from said sample material, said screen means being constructed of a material that permits the pattern displayed thereon to be viewed from a side of the screen means opposite said sample material, said screen means including an aperture therein through which said incident light beam is directed to illuminate said point on said sample material;
camera means positioned on the same side of said screen means as said light source means to record the pattern displayed on said screen means; and
microprocessor means coupled to said camera means for processing electrical signals received therefrom to provide a two-dimensional intensity distribution of the pattern recorded by said camera means, said two-dimensional intensity distribution being indicative of the periodic and diffractive microstructure characteristics of said sample material.
