Synthesis of large crystal size ZSM-5
AssigneeMobil Oil Corporation
InventorsFrancis G. Dwyer, Pochen Chu, William E. Cormier, Jr.
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Abstract
There is provided a method for making large crystal size ZSM-5. This method involves the use of two organic cations, specifically tetrapropylammonium (TPA) and tetramethylammonium (TMA) cations, in the reaction mixture. This method further involves the use of a source of deliberately added alumina, such as aluminum sulfate, in the reaction mixture.
Claims1
A method for preparing ZSM-5, said method comprising forming an aqueous reaction mixture comprising sources of silica, alumina, tetrapropylammonium cations and tetramethylammonium cations, wherein said reaction mixture includes a source of deliberately added alumina which is not an aluminum containing impurity from the other reactants and/or equipment used, and maintaining said reaction mixture under sufficient crystallization conditions until crystals of said ZSM-5 are formed.
Dependencies are inferred from the claim text.