Process for the preparation of 3-chloropropyl-silanes
AssigneeHuls Aktiengesellschaft
InventorsClaus-Dietrich Seiler, Willy Hange, Bernhard Lillig, Reinhard Matthes, Uwe Schon
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Abstract
3-chloropropylsilanes are prepared from hydrogensilanes and allyl chloride, where a stoichiometric excess of allyl chloride is maintained in the condensate of the vapor emitted by the boiling reactant mixture.
Claims2
Process for the preparation of a 3-chloropropylsilane from a hydrogensilane and allyl chloride at a temperature which is at least equal to the boiling point of the higher boiling point reactant, by subjecting the reactants to an addition reaction in the presence of a platinum-containing carrier material located above the reactant mixture, conducting the vapors of the reactant mixture to a condenser while bypassing the carrier material, and passing the condensate formed in the condenser through the carrier material by way of a sluice into the boiling reactant mixture, where the condensate formed in the condenser which flows over the carrier material contains a stoichiometric excess of allyl chloride, based on the hydrogen-silane reaction compound.
Dependencies are inferred from the claim text.