Composite abrasive compact having high thermal stability
AssigneeUS Synthetic Corporation
InventorsJohn Bunting, Bill Pope
Life of this patent
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Abstract
An abrasive compact with a substantially solid body is provided from a mass of abrasive particles which are bonded together on a particle-to-particle basis. A network of interstices is formed within the body by removing the metallic second phase by-product of a solvent catalyst sintering aid. The network of interstices is filled with the carbide by product of a non-catalyst sintering aid forking a solid body. A substrate is bonded to some of the particles and to some of the carbide filling the network of interstices.
Claims42
An abrasive compact having high thermal stability at temperatures above 700.degree. C. for cutting and drilling tools, said abrasive compact comprising:
- a plurality of abrasive particles bonded by a first sintering of said plurality of abrasive particles with a solvent-catalyst sintering aid in a first refractory metal cylinder at pressure of 55 to 72 k bars and at temperature of 1200.degree. C. to 2200.degree. C. in particle-to-particle contact at selected surface areas of said plurality of abrasive particles and from which said solvent-catalyst has been removed from between other surface areas of said plurality of abrasive particles which are spaced from each other for forming a network of interstices extending throughout said abrasive compact;
- and
- b) a binder matrix located in said network of interstices extending throughout said abrasive compact for filling said network interstices, said binder matrix generated by sintering, for a second time, said plurality of abrasive particles with a non-solvent catalyst sintering aid, in a second refractory metal cylinder at pressures of 55 to 72 K bars, at a temperature of 1200.degree. C. to 2200.degree. C. for bonding to at least some of said plurality of abrasive particles at said other surfaces areas.
An abrasive compact having high thermal stability at temperatures above 700.degree. C. for cutting and drilling tools, said abrasive compact comprising:
- a plurality of abrasive particles of irregular shape having selected surface areas of the respective particles bonded together in particle-to-particle contact by a first sintering of said plurality of abrasive particles with a solvent-catalyst sintering aid in a first refractory metal cylinder at pressure of 55 to 72 K bars at a temperature of 1200.degree. C. to 2200.degree. C.;
- b) a network of interstices throughout said abrasive compact formed by removing a metallic second phase from said abrasive compact formed by sintering said plurality of abrasive particles with said solvent-catalyst sintering aid;
- and,
- said network of interstices through said abrasive compact filled with a carbide generated by a second sintering of said plurality of abrasive particles with a non-solvent catalyst sintering aid, in a second refractory metal cylinder at pressure of 55 to 72 K bars at a temperature of 1200.degree. C. to 2200.degree. C.
A diamond compact comprising:
- a plurality of diamond crystals bonded directly to each other at selected areas of their surfaces by a first sintering of said plurality of diamond crystals with a solvent-catalyst sintering aid, under a pressure of 55 to 72 K bars and at a temperature of 1200.degree. C. to 2200.degree. C. for generating a metallic second phase within said plurality of diamonds, said plurality of diamond crystals spaced from each other at other areas of their said surfaces for defining a diamond mass with a network of interstices through said diamond mass;
- b) a network of interstices formed by removing said metallic second phase from said diamond mass;
- and
- said network of interstices filled with a carbide formed by a second sintering of said plurality of diamond particles with a non-solvent catalyst sintering aid under pressure of between 55 to 72 K bars and at a temperature of 1200.degree. C. to 2200.degree. C.
An abrasive compact having a substantially solid body having high thermal stability at temperatures above 700.degree. C. for cutting and drilling tools, said abrasive compact comprising:
- a plurality of abrasive particles bonded, at least in part, one to another along selected surface areas of adjacent particles such plurality of abrasive particles having been sintered in a first refractory metal cylinder in the presence of a solvent-catalyst sintering aid at pressures of 55 to 72 K bars and at a temperature of 1200.degree. C. to 2200.degree. C. a network of interconnected spaces defined by other surface areas of adjacent particles where said other surface areas of adjacent particles are spaced from each others;
- b) said network of interconnected spaces formed by removal of a metallic second phase from such interconnected spaces said metallic second phase having been an alloy of sao solvent-catalyst sintering aid:
- c) said network of interconnected spaces filled with a carbide generated by a second sintering of said plurality of abrasive particles in a second refractory metal cylinder in the presence of a non-solvent catalyst sintering aid at a pressure of between 55 to 72 K bars and at a temperature of 1200.degree. C. to 2200.degree. C.;
- and
- d) a substrate bonded to at least some surface areas of some abrasive particles and bonded to at least some said carbide for forming an essentially solid abrasive compact.
A process for preparing a high density abrasive compact having high thermal compact having high thermal stability at temperatures above 700.degree. C. for cutting and drilling tools comprising:
- a) sintering a mass of abrasive particles with a solvent catalyst sintering aid in a refractory metal cylinder at pressures of 55 to 72 K bars and at a temperature of 1200.degree. C. to 1600.degree. C. for ten minutes for forming a compact mass of interconnected abrasive particles with a metallic second phase;
- b) removing said compact mass from said refractory metal cylinder and removing said metallic second phase from said compact mass for creating a network of interconnected interstices throughout said compact mass;
- c) placing said compact mass in a refractory metal cylinder along with a layer of sintering aid material and a supporting substrate and sintering the combination in said cylinder at internal pressures of 55 to 65 K bars and at a temperature of 1200.degree. C. to 1600.degree. C. so that said sintering aid material infiltrates into said interconnecting interstices and said supporting substrate is bonded to said compact.
A process for preparing a high density abrasive tool compact for cutting and drilling tools comprising:
- a) placing a layer of abrasive particles and a solvent-catalyst in a refractory metal cylinder in preparation for sintering;
- applying pressure to said layer and said solvent-catalyst of 55 to 65 K bars and subjecting said layer and said solvent-catalyst to temperatures of 1200.degree. C. to 1600.degree. C. for a period of one to ten minutes for sintering said layer of abrasive particles into a compact abrasive mass with metallic second phase;
- c) removing said compact mass with metallic second phase from said refractory meal cylinder;
- d) removing said metallic second phase from said compact abrasive mass for creating a network of interconnecting interstices throughout said compact mass;
- e) placing said compact abrasive mass and a non-catalyst sintering aid material in a refractory metal cylinder in preparation for sintering;
- and
- f) applying pressure to said compact abrasive mass and said non-catalyst sintering aid material of 55 to 65 K bar and subjecting said compact mass and said non-catalyst sintering aid material to temperatures of 1200.degree. C. to 1600.degree. C. for driving said non-catalyst sintering aid material into said network of interconnected interstices for forming said tool compact.
Dependencies are inferred from the claim text.