# US 4,964,902 A · Method of extracting spin cast fused silica > Agents: this data is available as JSON from the patentgrep API and MCP server — see https://patentgrep.com/llms.txt - Number: US 4,964,902 A - Document ID: US4964902A - Status: Granted - Kind: A - Application number: 07/309,585 - Filed: 1989-02-10 - Granted: 1990-10-23 - Earliest claimed: 1989-02-10 - Assignees: Quartz & Silice - Inventors: Paul Guibert; Francis A. P. Launay - Web page: https://patentgrep.com/patent/US4964902A ## CPC - C03B 19/095: {by centrifuging, e.g. arc discharge in rotating mould (crucibles for crystal pulling in general C30B15/10, C30B35/002)} - C03B: MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES ## Abstract This invention relates to a method of making an object of silica glass, such as a crucible, according to which a pot capable of rotating about its axis is filled with a refractory pulverulent material. The pot is rotated and a cylindrical cavity is formed in the material, the axis of which coincides with that of the pot. The bottom and the wall of the cavity are then formed to a certain thickness with a silica-rich material. This silica-rich material is melted, the object thus produced is cooled and then extracted vertically by an extraction mechanism comprising a gripping member which is rotating, at least initially, at the same speed as the pot. ## Claims ### Claim 1 A method of making a fused silica glass object which comprises: filling a pot, capable of rotating about its axis, with pulverulent refractory material; rotating the pot to form a cavity having a uniform boundary in said pulverulent refractory material, the axis of said cavity coinciding with the axis of the pot, and introducing a fusible silica-rich glass forming material into said cavity to form an object having a bottom and a wall of a predetermined thickness; melting at least a portion of the thickness of said silica-rich glass forming material without melting said pulverulent refractory material to form a fused glass silica object; cooling the object thus produced; and extracting the object vertically, while the pot and object are rotating with an extraction mechanism which is rotating, at least initially, at the same speed as the pot. ### Claim 2 (depends on 1) The method of claim 1, wherein said object is extracted by gripping the object from above the pot while initially rotating said extraction mechanism at the same speed as that of the pot. ### Claim 3 (depends on 2) The method of claim 2, wherein the gripping of said object is accomplished by sealingly contacting the upper edge of said object with a gripping member, reducing the pressure within the zone defined by the interface between said object and said gripping member to secure said object to said gripping member, and raising the gripping member with the object adhered to it. ### Claim 4 (depends on 3) The method of claim 3, wherein said gripping member is raised slowly so as to cause minimum disturbance of said pulverulent refractory material. ### Claim 5 (depends on 3) The method of claim 3, wherein said gripping member is lowered vertically into said rotating pot such that a portion of said member contacts with the rim of said pot, thereby causing said member to rotate and wherein the the member is further lowered until it comes into bearing against the upper edge of the object. ### Claim 6 In a method for making a fused silica glass object in a rotating pot by filling the pot with a pulverulent refractory material, rotating the pot to form a cavity in said pulverulent material, introducing a fusible, silica-rich glass forming material into the cavity, melting said silica-rich glass forming material to form a fused silica object in the shape of said cavity and with an open interior portion, and cooling the silica glass object produced, the improvement which comprises removing the fused silica glass object from said cavity by extracting the object vertically while the pot and object are rotating while sealingly contacting the upper edges of said object with a rotating gripping member; reducing the pressure between said object and said gripping member to secure said object to said gripping member, and raising the rotating gripping member with the object adhered to it at a rate which causes minimum disturbance to the pulverulent refractory material. ### Claim 7 A method of making a fused silica glass object which comprises: filling a pot, capable of rotating about its axis with pulverulent refractory material; rotating the pot to form a cavity having a uniform boundary in said pulverulent refractory material, the axis of said cavity coinciding with the axis of the pot, and introducing a fusible silica-rich glass forming material into said cavity to form an object having a bottom and a wall of a predetermined thickness; melting at least a portion of the thickness of said silica-rich glass forming material without melting said pulverulent refractory material to form a fused silica glass object, said object having an interior portion said portion coinciding with the axis of the pot; cooling the object thus produced; releasably contacting said object while the pot and object are rotating with an extraction mechanism which is rotating, at least initially, at the same speed as the pot; and extracting the object by vertically raising said extraction mechanism. ### Claim 8 (depends on 7) The method of claim 7, wherein said object is extracted by releasably gripping the object from above the pot. ### Claim 9 (depends on 8) The method of claim 8, wherein the gripping of said object is accomplished by sealingly contacting the upper edge of said object with a gripping member, reducing the pressure within the zone defined by the interface between said object and said gripping member to secure said object to said gripping member, and raising the extraction mechanism with the object adhered to the gripping member. ### Claim 10 (depends on 9) The method of claim 9 wherein the pressure in the interior portion of the object is reduced by connecting duct means for generating a vacuum through said extraction member and in communication with the interior portion of said object. ### Claim 11 (depends on 9) The method of claim 9, wherein said gripping member is raised slowly so as to cause minimum disturbance of said pulverulent refractory material. ### Claim 12 (depends on 11) The method of claim 11, wherein said gripping member is lowered vertically into said rotating pot such that a portion of said member contacts with the rim of said pot, thereby causing said member to rotate and wherein the member is further lowered until it comes into bearing against the upper edge of the object. ### Claim 13 (depends on 12) The method of claim 12, which further comprises aligning the axis of said extraction member with the axis of said pot. ### Claim 14 (depends on 13) The method of claim 13 wherein said aligning step is effectuated by providing said extraction member with a rotational synchronization member which assures contact with the outer edge of said pot. ### Claim 15 (depends on 14) The method of claim 14 wherein said aligning step includes engaging said outer edge of the pot with said rotational synchronization member by spring means. ### Claim 16 (depends on 15) The method of claim 15 wherein the pressure in the interior portion of the object is reduced by connecting duct means for generating a vacuum through said extraction member and in communication with the interior portion of said object.