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US 4,900,411 AGranted
Method of preparing a high-purity polycrystalline silicon using a microwave heating system in a fluidized bed reactor
AssigneeKorea Research Institute of Chemical Technology
InventorsYoon Poong, Song Yongmok
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Abstract
Method and apparatus for the preparation of high-purity polycrystalline silicon deposited by thermal decomposition or hydrogen reduction of a gaseous halogenated silicon on high-purity silicon particles in a fluidized bed reactor heated by microwave.
Claims14
A method for preparing polycrystalline silicon comprising:
- supplying silicon seed to a single-column fluidized bed reactor to form a bed of silicon seed particles;
- introducing and dispersing a silicon-containing reacting gas into the reactor through a gas distribution means arranged below said bed to fluidize the silicon seed;
- heating the silicon seed above said gas distribution means by introducing microwave energy from at least one side of the reactor into a lower reaction zone of the reactor to deposit silicon from the silicon-containing reacting gas onto the silicon seed to form polycrystalline particles;
- introducing a coolant fluid into said gas distribution means;
- and
- cooling said gas distribution means with said coolant fluid to maintain said gas distribution means at a temperature to prevent substantial deposition of silicon on said gas distribution means.
3 more elements
Dependencies are inferred from the claim text.