# US 4,889,591 A · Crotalaria juncea paper pulps > Agents: this data is available as JSON from the patentgrep API and MCP server — see https://patentgrep.com/llms.txt - Number: US 4,889,591 A - Document ID: US4889591A - Status: Granted - Kind: A - Application number: 07/199,804 - Filed: 1988-05-27 - Granted: 1989-12-26 - Earliest claimed: 1988-05-27 - Assignees: Process Evaluation and Development Corporation - Inventors: Eduardo J. Villavicencio; Camilo Gomez-Estevez - Web page: https://patentgrep.com/patent/US4889591A ## CPC - D21B 1/025: {Separating pith from fibrous vegetable materials} - D21C 3/02: with inorganic bases or alkaline reacting compounds, e.g. sulfate processes - D21B: FIBROUS RAW MATERIALS OR THEIR MECHANICAL TREATMENT - D21C: PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR ## Abstract The present process produces a long fiber suitable for making various paper products. The long fiber is derived from Crotalaria juncea. The processing consists of a particular technique for preparing the fiber for digestion and a particular digestion sequence. In the preparation of the fiber for digestion it is dried to less than about 30 percent moisture, moist depithed, washed and wet depithed. The fiber is then processed at a high caustic concentration using a sequence of digestion-pressure reduction-digestion. Optionally there can be a third stage of digestion with a pressure reduction prior to the digestion. After digestion has been completed the fiber is refined and sent to blowdown. The fiber is then screened, washed and bleached. The resulting long fiber will product a high quality paper or is admixed with short fibers and various paper products can be made. ## Claims ### Claim 1 A method for producing a paper pulp using Crotalaria juncea as the primary source of long fiber comprising: a. harvesting said Crotalaria juncea; b. reducing the moisture content of the Crotalaria juncea to less than about 30 percent by weight; c. reducing the size of the pieces of said Crotalaria juncea to smaller fragments; d. shredding and depithing said Crotalaria juncea at its ambient moisture level; e. washing the depithed Crotalaria juncea; f. wet depithing the washed Crotalaria juncea; g. contacting the washed and depithed Crotalaria juncea fibers with an aqueous solution comprising sodium hydroxide containing at least about 8 percent by weight sodium hydroxide at a temperature of greater than about 180.degree. C. for a first period of time; h. rapidly reducing the pressure at least about 1 kg/cm.sup.2 with a resulting reduction of temperature and continuing the contact of said Crotalaria juncea fibers with said aqueous sodium hydroxide for a second period of time; and i. recovering a Crotalaria juncea paper pulp. ### Claim 2 (depends on 1) A method for producing a paper pulp using Crotalaria juncea as the primary source of long fibers as in claim 1 wherein the moisture content of said Crotalaria juncea is reduced to about 20 percent by weight prior to being reduced in size. ### Claim 3 (depends on 1) A method for producing a paper pulp using Crotalaria juncea as the primary source of long fiber as in claim 1 wherein the concentration of sodium hydroxide on said Crotalaria juncea fibers is about 10 percent by weight to about 35 percent by weight. ### Claim 4 (depends on 1) A method for producing a paper pulp using Crotalaria juncea as the primary source of long fiber as in claim 1 wherein during the contacting of said Crotalaria juncea with sodium hydroxide for a first period of time said temperature is maintained at about 190.degree. C. to 200.degree. C. ### Claim 5 (depends on 4) A method for producing a paper pulp using Crotalaria juncea as the primary source of long fiber as in claim 4 wherein during continuing contact of Crotalaria juncea with sodium hydroxide for a second period of time said temperature is about 175.degree. C. to 185.degree. C. ### Claim 6 (depends on 1) A method for producing a paper pulp using Crotalaria juncea as the primary long fiber source as in claim 1 wherein prior to continuing the contact of said Crotalaria juncea with sodium hydroxide for a second period of time said Crotalaria juncea is processed in a refiner. ### Claim 7 (depends on 1) A method for producing a paper pulp using Crotalaria juncea as the primary long fiber source as in claim 1 wherein after said Crotalaria juncea is processed in a refiner said Crotalaria juncea is washed, screened and bleached. ### Claim 8 (depends on 1) A method for producing a paper pulp using Crotalaria juncea as the primary long fiber source as in claim 1 wherein a pulp consisting primarily of short fibers is admixed with said Crotalaria juncea pulp. ### Claim 9 (depends on 8) A method for producing a paper pulp using Crotalaria juncea as the primary long fiber source as in claim 8 wherein said Crotalaria juncea fibers comprise from about 2 weight percent to about 35 percent by weight of the fiber content of the admixed pulp. ### Claim 10 (depends on 9) A method for producing a paper pulp using Crotalaria juncea as the primary source of long fibers as in claim 9 wherein said Crotalaria juncea fibers comprise from about 5 percent by weight to about 20 percent by weight of the fiber content of the admixed pulp. ### Claim 11 (depends on 9) A method for producing a paper pulp using Crotalaria juncea as the primary source of long fibers as in claim 9 wherein said pulp consisting primarily of short fibers is selected from the group consisting of bagasse pulp, hardwood pulp and straw pulp. ### Claim 12 (depends on 1) A method for producing a paper pulp using Crotalaria juncea as the primary source of long fibers as in claim 1 wherein the contact of said Crotalaria juncea with said aqueous sodium hydroxide is for periods of time greater than about 15 minutes. ### Claim 13 (depends on 1) A method for producing a paper pulp using Crotalaria juncea as the primary source of long fibers as in claim 1 wherein a fiber source that yields short fibers after digestion is admixed with said Crotalaria juncea prior to depithing. ### Claim 14 (depends on 13) A method for producing a paper pulp using Crotalaria juncea as the primary source of long fibers as in claim 13 wherein said fiber source that yields short fibers is selected from the group consisting of bagasse, straw and hardwoods. ### Claim 15 (depends on 14) A method for producing a paper pulp using Crotalaria juncea as the primary source of long fibers as in claim 14 wherein said fiber source is bagasse. ### Claim 16 (depends on 13) A method for producing a paper pulp using Crotalaria juncea as the primary source of long fibers as in claim 13 wherein said fiber source that yields short fibers is present in a concentration of about 2 percent by weight to about 30 percent by weight. ### Claim 17 (depends on 16) A method for producing a paper pulp using Crotalaria juncea as the primary source of long fibers as in claim 16 wherein the concentration of said fiber source that yields short fibers is about 5 percent by weight to about 30 percent by weight. ### Claim 18 (depends on 1) A paper pulp comprised of from about 2 percent by weight to about 35 percent by weight Crotalaria juncea according to claim 1 and from about 65 percent by weight to about 98 percent by weight of a short fiber source. ### Claim 19 (depends on 18) A paper pulp as in claim 18 wherein said short fiber source is selected from the group consisting of bagasse, straw and hardwoods. ### Claim 20 A method for preparing Crotalaria juncea for digestion comprising: a. harvesting said Crotalaria juncea; b. reducing the moisture content of the Crotalaria juncea to less than about 30 percent by weight; c. reducing the size of the pieces of said Crotalaria juncea to smaller fragments; d. shredding and depithing said Crotalaria juncea at its ambient moisture level; e. washing the depithed Crotalaria juncea; and f. wet depithing the washed Crotalaria juncea.