Liquid-vapor contact method and apparatus
AssigneeThe BOC Group, Inc.
InventorDavid C. F. Gladman
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AssigneeThe BOC Group, Inc.
InventorDavid C. F. Gladman
Estimating the term…
In a distillation column used in the separation of air, a liquid stream of composition intermediate those occuring at the top and bottom is taken from the column and is at least partial reboiled in an external heat exchanger by heat exchange with a heat exchange fluid. The resultant vapor is returned to the column. Its composition matches that of the vapor in the vapor space to which it is returned more closely than that of the vapor in the vapor space above the tray from which the liquid is taken for reboil. The heat exchange fluid is other than one which is taken from a liquid vapor contact column, is passed directly to the heat exchanger, and is then returned directly to the column from which it was taken. The distillation column is preferably the lower pressure column of a double column system, and the heat exchange fluid is preferably air which preferably condenses in the heat exchanger and is introduced into the column at a level above that from which the liquid stream of intermediate composition is taken.
A method of distilling air in at least one liquid-vapor contact column in which a boiling liquid phase comprising a mixture of oxygen, nitrogen and argon is contacted intimately and undergoes mass exchange with a condensing vapor phase comprising oxygen, nitrogen and argon, said method including the steps of:
Apparatus for distilling air, comprising a first liquid vapor contact column in which, in use, a boiling liquid phase comprising oxygen, nitrogen and argon is contacted intimately and undergoes mass exchange with a condensing vapor phase comprising oxygen, nitrogen and argon, said first column having at least one outlet passage at a chosen level for the withdrawal of a liquid stream of composition intermediate the extremes of composition that obtain in the column, in use, and communicating with heat exchange means operable to boil at least part of said stream by heat exchange with heat exchange fluid, wherein the said heat exchange means is external to the column and is in communication with said column or another liquid vapor contact column at a level such that a stream of boiled liquid mixes with vapor and such that the composition of the returning stream matches more closely the composition of the vapor with which it is mixed, in use, than it does the composition of the vapor in mass exchange with the liquid at said chosen level, there being a path for the flow of said heat exchange fluid, other than one in which, in use, the heat exchange fluid passes directly from one liquid-vapor contact column, undergoes phase change in heat exchange relationship with said intermediate composition stream, and returns directly to the same column.
Dependencies are inferred from the claim text.