Homogeneous mixtures of polyphosphates
AssigneeOccidental Chemical Corporation
InventorJohn A. Peterson
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Abstract
A homogeneous, particulate mixture of alkali metal pyrophosphates and tripolyphosphates is prepared by flash drying an aqueous solution of alkali metal orthophosphates having an alkali metal to phosphorus mole ratio in the range of 5:3 to 6:3, and calcining the resultant dried particles. Preferably, the alkali metal is sodium and the orthophosphate solution is adjusted to provide a major proportion of sodium pyrphosphate and a minor proportion of sodium tripolyphosphate in the final product.
Claims1
A process for preparing a homogenous, particulate mixture of sodium pyrophosphate and sodium tripolyphosphate, said process consisting essentially of the steps of:
- (a) forming an aqueous solution of monosodium phosphate and disodium phosphate having a sodium to phosphorus mole ratio in the range of from 5:3 to 6:3,
- (b) flash drying the solution at a temperature in the range of from about 150.degree. C. to about 250.degree. C. to form phosphate particles,
- (c) calcining the dried particles at a temperature of from about 350.degree. C. to about 550.degree. C. to convert monosodium phosphate and disodium phosphate particles into homogenous polyphosphate particles, and
- (d) recovering said homogenous polyphosphate particles, said particles containing from about 75% to about 85% by weight of sodium pyrophosphate and from about 15% to about 25% by weight of sodium tripolyphosphate.
Dependencies are inferred from the claim text.