Method for preparing 3-ethylbenzophenone
AssigneeNippon Petrochemicals Company, Limited
InventorsIsoo Shimizu, Yasuo Matsumura, Shigenobu Kawakami, Atsushi Sato
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AssigneeNippon Petrochemicals Company, Limited
InventorsIsoo Shimizu, Yasuo Matsumura, Shigenobu Kawakami, Atsushi Sato
Estimating the term…
The present invention provides a method for preparing 3-ethylbenzophenone in a high purity which comprises the steps of alkylating benzene with ethylene with the aid of an alkylating catalyst to obtain an alkylated product composed mainly of unreacted benzene, ethylbenzene, polyethylbenzenes and heavier by-products; subjecting the alkylated product to distillation in order to recover therefrom a fraction which has a temperature range of boiling points within the range of 275.degree. to 310.degree. C. (in terms of atmospheric pressure); dehydrogenating the recovered fraction at a reaction temperature within the range of 200.degree. to 700.degree. C. in the presence of a dehydrogenating catalyst; oxidizing the dehydrogenated fraction in a liquid phase; and performing distillation to recover therefrom 3-ethylbenzophenone represented by the formula: ##STR1##
A method for preparing 3-ethylbenzophenone in a high purity which consists essentially of the steps of alkylating benzene with ethylene in the presence of an alkylating catalyst comprising aluminum chloride at a temperature within the range of about 0.degree. to 175.degree. C. to obtain an alkylated product composed mainly of unreacted benzene, ethylbenzene, polyethylbenzene and heavier substances;
A method for preparing 3-ethylbenzophenone in a high purity which consists essentially of the steps of alkylating benzene with ethylene in the presence of an alkylating catalyst comprising aluminum chloride at a temperature within the range of about 0.degree. to 175.degree. C. to obtain an alkylated product composed mainly of unreacted benzene, ethylbenzene, polyethylbenzene and heavier substance;
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