Rocket nozzles in layered construction

A process to produce a rocket nozzle, whose inside surface guides a gas stream, and is formed by a liner made from a carbide material according to the following steps:

• A--a powder, comprising silicon carbide crystals, carbon and a binder material is isostatically pressed into a thin walled body of rotation with the shape of a liner (2) having a converging portion, a neck portion and a diverging portion,
• B--said body of rotation is converted to silicon carbide by siliconization in a reaction-sintering process, forming said liner (2),
• C--the liner (2) is kept under vacuum at a temperature above 1400 C to vaporize the majority of free silicon,
• D--a layer of highly anisotropic graphite, the surface of which is normal to the vectorial direction of the lowest ultimate compression strength of said graphite, forms a jacket (3) around the outer surface of the liner (2) permitting thermal expansion of the liner (2) during rocket operation, said layer being applied sufficiently thick in order to be able to absorb said thermal expansion,
• E--a thick layer of a heat resistant material such as phenolic graphite is arranged around the outer surface of the jacket (3) forming a third layer,
• F--the thin walled liner (2), with the jacket (3) and the third layer is heated in an inert atmosphere until the thick layer hardens and forms a shell (7).

A process to produce a rocket nozzle, whose inside surface guides a gas stream, and is formed by a liner made from a carbide material according to the following steps:

• A--a powder, comprising silicon carbide crystals, carbon and a binder material is isostatically pressed into a thin walled body of rotation with the shape of a liner (2) having a converging portion, a neck portion and a diverging portion,
• B--said body of rotation is converted to silicon carbide by siliconization in a reaction-sintering process, forming said liner (2),
• C--the liner (2) is kept under vacuum at a temperature above 1400 C to vaporize the majority of free silicon,
• D--the outer surface of the liner (2) is exposed to a pyrolysis treatment to produce crystal growth in a direction that results in anisotropic distribution of the lowest ultimate compression strength, the vectorial direction of the lowest ultimate compression strength being normal to the outside surface of the liner, this treatment being applied until the thickness of the deposition, which forms a jacket (3) consisting of anisotropic crystals, permits thermal expansion of the liner (2) because of the low ultimate compression strength of the jacket (3) in a direction normal to the outside surface of the liner (2), permitting a sufficient reduction of the thickness of the jacket (3) under the pressure of the forces of the thermal expansion of the liner (2) during operation of the rocket,
• E--a thick layer of a heat resistant material such as phenolic graphite is arranged around the outer surface of the jacket (3) forming a third layer,
• F--the thin walled liner (2), with the jacket (3) and the third layer are heated in an inert atmosphere until the thick layer hardens and forms a shell (7).