US 4,696,799 AGranted

Ammonia synthesis converter

AssigneeThe M. W. Kellogg Company

InventorStephen A. Noe

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Abstract

A horizontal, cold wall, multi-bed ammonia converter having two, shell and tube interchangers for cooling reaction gas streams leaving respectively the first and second catalyst beds with incoming reactant gases wherein each of the interchangers is vertically oriented and physically located between catalyst beds. The catalyst beds are adiabatic, slab-shape beds defined in part by side portions of the inner wall of the converter and are arranged for downward, transverse flow of reacting gases. Longitudinal conduits and baffling in cooperation with the arrangement of catalyst beds and interchangers provide serial flow of gas through the cold side of each of the interchangers, a first catalyst bed, the hot side of one of the interchangers, a second catalyst bed, the hot side of the other interchanger, a third catalyst bed, and, optionally, a fourth catalyst bed.

A horizontal ammonia converter having a first end and a second end which comprises:

(a) a cylindrical pressure shell having outer heads contiguous therewith at the first and secodn ends;
(b) a cylindrical inner shell disposed within substantially the entire length of the pressure shell and defining a shell annulus therewith, the inner shell having first and second end closures contiguous with the cylindrical inner shell, the first end outer head defining a first gas plenum with the first end closure and the second end outer head defining a second gas plenum with the second end closure;
(c) gas inlet means disposed in the second end outer head in serial fluid communication with the second gas plenum, the shell annulus, and the first gas plenum;
(d) gas outlet means;
(e) first, second, and third, slab-flow catalyst beds defined by transverse bulkheads within the inner shell and opposed side portions of the inner shell, the first catalyst bed being proximate the first end of the converter and the second catalyst bed being spaced between the first and third catalyst beds, each of the catalyst beds having a top inlet face and a bottom outlet face;
(f) a first heat exchanger having an upper end and vertical U-tubes with inlet and outlet means at the upper end of the exchanger, the first heat exchanger being disposed between the first and second catalyst beds;
(g) a second heat exchanger having vertical tubes with inlet and outlet means, the second heat exchanger being disposed between the second and third catalyst beds;
(h) first longitudinal conduit means disposed within the cylindrical inner shell below and externally proximate to the first and second catalyst beds providing fluid communication between the first gas plenum and the inlet means of the second heat exchanger;
(i) second longitudinal conduit means disposed within the cylindrical inner shell above and externally proximate to only the second catalyst bed providing fluid communication between the outlet means of the second heat exchanger and the inlet means of the first heat exchanger;
(j) baffle means for conducting gas successively from the outlet means of the first heat exchanger downwardly through the first catalyst bed, across tube exteriors of the first heat exchanger, downwardly through the second catalyst bed, across tube exteriors of the second heat exchanger and downwardly through the third catalyst bed;
and
(k) means for conducting gas from the bottom outlet face of the third catalyst bed to the gas outlet means.

9 more elements

Abstract

Claims3