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US 4,645,512 AGranted
Continuous process for removing water-soluble particles from organic liquids
AssigneeThe Dow Chemical Company
InventorDennis M. Johns
Life of this patent
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Abstract
A process for the removal of water-soluble particles from a heavier-than-water organic liquid which easily emulsifies with water, comprising conducting a countercurrent extraction with water in a vertical extraction zone wherein an organic phase is maintained as a continuous phase and the water migrates upwardly through the organic liquid as a disperse phase.
Claims8
A method for removing finely divided, water-soluble particles from a heavier-than-water water insoluble organic liquid containing the particles suspended therein, which liquid readily forms an emulsion with water, comprising:
- (a) introducing into an extraction zone containing therein a body of the organic liquid as a lower discrete layer and a body of water as an upper discrete layer thereover, a stream of the organic liquid containing the water-soluble particles suspended therein into an upper portion of the body of the organic liquid;
- (b) introducing a stream of water into a lower portion of the body of the organic liquid in the extraction zone as a discontinuous phase therein;
- and
- (c) withdrawing water from an upper portion of the extraction zone and withdrawing from a bottom portion of the extraction zone the organic liquid from which at least a portion of the particles have been removed, at respective rates which maintain a liquid-liquid interface between the body of water and the body of liquid in the upper portion of the extraction zone;
- wherein said organic liquid is introduced and maintained as a continuous, non-dispersed phase and said stream of water is maintained as a dispersed phase while in the organic liquid;
- whereby water passes through the body of the organic liquid in countercurrent relationship thereto and dissolves said water soluble particles therein while passing therethrough.
3 more elements
Dependencies are inferred from the claim text.