Process for the preparation of silica spheres
AssigneeShell Oil Company
InventorsMadjid Afghan, Josephus G. Sponselee
Life of this patent
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Abstract
Silica spheres are prepared in a process comprising: (a) preparing a silica hydrosol by mixing an aqueous solution of an alkali metal silicate with an aqueous solution of an acid; (b) converting the hydrosol into droplet form; (c) aging the droplets in a fluid to produce hydrogel particles; (d) partially drying the hydrogel particles at 10.degree. to 60.degree. C. in air having a relative humidity in the range of from 45 to 95%, to a water content in the range of from 0.3 to 1.3 kg/kg solids; (e) decreasing the cation content of the hydrogel particles by ion-exchange in an aqueous medium to less than 10% w, calculated on dry material; and (f) finally drying the hydrogel particles to obtain silica spheres.
Claims15
A process for the preparation of silica spheres which comprises:
- (a) preparing a silica hydrosol by mixing an aqueous solution of an alkali metal silicate with an aqueous solution of an acid;
- (b) converting the hydrosol into droplet form;
- (c) aging the droplets in a fluid to produce hydrogel particles;
- (d) partially drying the hydrogel particles at 10.degree. to 60.degree. C. in air having a relative humidity in the range of from 45 to 95%, to a water content in the range of from 0.3 to 1.3 kg/kg solids;
- (e) decreasing the cation content of the hydrogel particles by ion-exchange in an aqueous medium to less than 10%w, calculated on dry material;
- and
- (f) finally drying the hydrogel particles to obtain silica spheres.
Dependencies are inferred from the claim text.