Method for controlling batch alkaline pulp digestion in combination with continuous alkaline oxygen delignification
AssigneeMannbro Systems Handelsbolag
InventorNils V. Mannbro
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AssigneeMannbro Systems Handelsbolag
InventorNils V. Mannbro
Estimating the term…
A method for batch pulp digestion with hydroxide-bearing cooking liquors in combination with continuous alkaline oxygen delignification is described. The brown stock washing plant and the connected oxygen stage are freed from oxygen-consuming black liquid by withdrawing black liquor from a pre-cook wherein cooking liquor is reacted with a surplus of hydroxide-consuming chips. Moreover, spent cooking liquor in the brown stock washing plant is displaced with spent liquor from the oxygen delignification stage (oxy-liquor) and/or alkalization spent liquor (bleaching spent liquor worth recovering because of its sodium content). A mixture of said liquors is prepared in a pressurized cooking liquor accumulator and charged to the digestion plant liquor circulation system. The cooking liquor's content of hydroxide for lignin release is continuously replenished by means of white liquor dosage which also compensates the dilution which is caused by the supply of oxy-liquor and other bleaching spent liquors whose hydroxide content reflects variations in the preceding digesting conditions pertaining to the cooking liquor and resulting Kappa number fluctuations.
In a method for batch pulp digestion of lignocellulose material with a hydroxide-bearing cooking liquid, in combination with continuous alkaline oxygen delignification comprising an oxygen-alkali process in subsequent pulp bleaching in a sequence of one or several steps, from which oxygen-alkali waste liquor having sodium compounds worth recovering and dissolved combustible lignin products is recovered via a brown stock washing step in such a way that oxygen-alkali waste liquor joins black liquor which is obtained by pulping of the material to a predetermined Kappa number, said pulping being controlled in part by the chemical charge to a predetermined hydroxide concentration in the cooking liquor and in part by the H-factor so that the subsequent oxygen delignification comprising said oxygen-alkali process can take place with small cellulose degradation and to the greatest extent constant composition of the recovered oxygen-alkali waste liquor comprising said oxygen-alkali waste liquor, pulping the lignocellulose material in a plurality of intermittent digesters using the hydroxide-bearing cooking liquor containing oxygen-consuming substances to produce brown stock, batchwise removing raw brown stock from said digesters, washing said raw brown stock with waste liquor from the oxygen-alkali process, contacting said washed brown stock with oxygen to effect oxygen delignification of said brown stock thereby to produce oxygen-alkali bleached pulp, removing oxygen-alkali waste liquor from said bleached pulp, using a first portion of the last-named waste liquor as said waste liquor in said raw brown stock washing step, removing a first portion of spent black liquor containing oxygen-consuming substances from said digesters and regenerating the same to produce hydroxide-bearing white liquor, feeding a second portion of said spent black liquor to a cooking liquor accumulator common to said plural digesters, feeding a second portion of said oxygen-alkali waste liquor to said cooking liquor accumulator, feeding a portion of said white liquor to said cooking liquor accumulator, measuring the hydroxide concentration by continuous analysis of said cooking liquor of said accumulator, and controlling the dosage of said white liquor to said accumulator in response to said hydroxide concentration measurement so as to maintain the hydroxide concentration of said cooking liquor substantially constant and to maintain a low value of the ratio
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