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US 4,575,551 AGranted
Acidic heteropolysaccharide AM-2
AssigneeNakano Vinegar Co., Ltd.
InventorsSeiichi Fujiyama, Hiroyuki Minakami, Kenji Tayama, Hiroshi Masai
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Abstract
Novel highly viscous acidic heterpolysaccharide AM-2 is produced from a strain of genus Acetobacter isolated from vinegar mash, and is useful as an adhesive, coating agent, drilling mud additive, enhanced oil recovering agent, etc., as well as a material useful for the production of foods, drugs and cosmetics because of its safety and high viscosity.
Claims1
Acidic heteropolysaccharide AM-2 having the following physiochemical characteristics:
- (1) composition
- composed of glucose, rhamnose, mannose, glucuronic acid and acetyl group as main components, the molar ratio of glucose:rhamnose:mannose:glucuronic acid being 4:0.9.about.1.1:0.9.about.1.1:0.9.about.1.1 and the acetyl group content is 4 to 8%;
- (2) infrared spectrum
- the infrared spectrum is as shown in FIG. 1;
- (3) color reaction
- Anthrone reaction:
- positive
- Carbazole reaction:
- positive
- Elson-Morgan's reaction:
- negative
- Iodine reaction:
- positive;
- (4) solubility in solvents
- soluble in water, and insoluble in ethanol, ether, acetone;
- (5) color and appearance
- the purified polysaccharide is white, cottony or fibrous;
- (6) viscosity
- the aqueous solution is colorless, transparent and viscous, and the viscosity of 1% solution is 1200 to 2000 cps as determined with a torque measuring viscometer at 25.degree. C. and a rate of 30 rpm;
- (7) elemental analysis:
- C:
- 39.9.+-.1%;
- H:
- 6.2.+-.1%;
- N:
- 0%;
- ash:
- 3.0.+-.1.0%;
- (8) Specific rotation
- [.alpha]sub.D.sup.27 =0.about.+20
- (C=0.33 in the aqueous solution);
- (9) molecular weight
- about 10.sup.5 or above;
- (10) melting point
- the polysaccharide turns dark brown at 190.degree. C. and decomposes at 250.degree. C.;
- and
- (11) nuclear magnetic resonance spectrum
- the .sup.13 C-nuclear magnetic resonance spectrum is as shown in FIG. 7.
35 more elements
Dependencies are inferred from the claim text.