Process for improving the flowability and increasing the bulk density of high-surface area valve metal powders
AssigneeHermann C. Starck Berlin
InventorsWolf-Wigand Albrecht, Axel Hoppe, Uwe Papp, Rudiger Wolf
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Abstract
The invention relates to an improvement of the flowability and an increase in the bulk density of high-surface area valve metal powders by means of the addition of finely divided extraneous metal oxides in quantities of up to 5000 ppm, relative to the quantity of metal, before the powder-metallurgical processing of the valve metal powder.
Claims18
Process for improving the flowability and increasing the bulk density of a high-surface area valve metal powder of capacitor quality suitable for being subjected to powder-metallurgical processing by compacting and sintering to produce a sintered anode, which comprises admixing with said valve metal power an additive for increasing the flow properties and bulk density of the valve metal powder, said additive consisting essentially of finely divided extraneous metal oxide in a quantity of up to 5000 ppm (relative to the quantity of metal) before the powder-metallurgical processing of the valve metal powder, said extraneous metal oxide being amorphous pyrogenic silica, aluminum oxide, talc powder, magnesium oxide or a combination thereof, or the combination of titanium dioxide and one or more of said other extraneous metal oxides.
Process for preparing a sintered anode which comprises compressing and sintering a high-surface area valve metal powder of capacitor quality, wherein said valve metal powder subjected to said compressing and sintering is admixed with an additive for increasing the flow properties and bulk density of the valve metal powder, said additive consisting essentially of finely divided extraneous metal oxide present in a quantity of up to 5000 ppm (relative to the quantity of metal), said extraneous metal oxide being amorphous pyrogenic silica, aluminum oxide, talc powder, magnesium oxide or a combination thereof, or a combination of titanium dioxide with one or more of said other extraneous metal oxides.
Dependencies are inferred from the claim text.