Continuous preparation of nylon with diamine recycling
AssigneeBASF SE
InventorsFranz Schmidt, Gunter Pipper, Josef G. Floss, Franz Zahradnik
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AssigneeBASF SE
InventorsFranz Schmidt, Gunter Pipper, Josef G. Floss, Franz Zahradnik
Estimating the term…
Nylons are prepared by a continuous process in which, in an evaporator zone, an aqueous solution of a salt of a dicarboxylic acid of 6 to 18 carbon atoms and a diamine of 6 to 18 carbon atoms is heated to 250.degree.-300.degree. C. under superatmospheric pressure, with simultaneous vaporization of water and formation of a prepolymer, the prepolymer and the vapors are separated continuously, the vapors are rectified and the entrained diamines are recycled, and the prepolymer is fed to a polycondensation zone and subjected to polycondensation under superatmospheric pressure of from 1 to 10 bar and at from 250.degree. to 300.degree. C., wherein the aqueous salt solution is heated under superatmospheric pressure of from 1 to 10 bar during a residence time of less than 60 seconds, with the proviso that, on leaving the evaporator zone, the degree of conversion is not less than 93% and the water content of the prepolymer is not more than 7% by weight.
A process for the continuous preparation of a nylon, which comprises
A process for the preparation of a nylon, which comprises
Dependencies are inferred from the claim text.