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AssigneeHoechst Aktiengesellschaft
InventorsBen Damman, Jan Drijver, Hans Kinneging, Hans Scheffer, Jaap Stam, Paul de Witte
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The disclosure relates to a process for making alkali metal phosphates, especially alkali metal polyphosphates, from alkali metal phosphate solutions or suspensions. To this end the solutions or suspensions are forced to flow through a plurality of single opening nozzle structures under a pressure of 6 to 66 bars and sprayed inside a tower through a flame zone produced by a plurality of burners arranged in annular fashion. The disclosure also relates to a device for carrying out the process, wherein a cylindrical spray tower (1) having a tapered lower end and being closed by means of a cover (2) has a solvent feed pipe (5) terminating in a spray means (6) centrally passed through the cover, and wherein a plurality of burners is passed through the cover (2), concentrically around the solvent feed pipe (5). The spray means (6) is comprised of a feed pipe (15) and at least one spray head (12), which has a plurality of single opening nozzle structures (17) disposed in its terminal surface area (13). At least one pressure-increasing pump ( 7) is disposed in the solvent feed pipe (5).
In a process for making alkali metal phosphates or alkali metal polyphosphates from feed materials selected from solutions and suspensions of alkali metal phosphates by introducing the feed materials in the upper portion of a spray tower, spraying them inside said spray tower through a flame zone produced by a plurality of burners arranged in annular fashion and collecting the dried alkali metal phosphates or metal polyphosphates, the improvement which comprises putting the feed materials under a pressure of 10 to 66 bars by means of at least one pressure-increasing pump;
Dependencies are inferred from the claim text.