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US 4,486,474 AGranted
Method of sizing strands
AssigneeThe Goodyear Tire & Rubber Company
InventorWilliam J. Hampshire
Life of this patent
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Abstract
A method of sizing a filament in the form of a mat of strand filament wound into a roll by immersing the roll in a ketone solvent containing an unsaturated epoxy resin and polyamine curative therefor followed by removing said ketone under vacuum conditions to unblock said polyamine and allowing it to partially cross-link said epoxy.
Claims9
A method of sizing a filament which comprises the steps of
- A. Immersing a mat of continuous strand filament wound into the form of a roll in a liquid ketone solvent solution containing less than a saturation amount of unsaturated epoxy resin and polyamine cross-linking curative therefor in a container with a vapor space above said solution, where said ketone chemically blocks said polyamine from crosslinking said epoxy resin.
- B. Soaking the immersed filament roll in said solution at substantially atmospheric pressure until the said roll is substantially saturated with said solution.
- C. Applying a vacuum to said vapor space, to remove residual air and thereby more completely saturate said roll with said solution.
- D. Removing the vacuum separating said roll from said solution, and placing said roll in a suitable container.
- E. Applying a vacuum to said suitable container to remove residual ketone solvent from the roll, thereby unblocking said polyamine curative and allowing the curative to partially cross-link said epoxy on said filament to a "B" stage cure.
- F. Removing said vacuum and recovering the roll of sized strand filaments having a partially crosslinked epoxy coating thereon in an amount of about 0.5 to about 15 weight percent of the filament and
- G. Cooling said roll of sized filament to at least 10.degree. C. to stop the crosslinking reaction.
4 more elements
Dependencies are inferred from the claim text.