Process for enhancing the fragrance qualities of ethylene glycol monoaryl ethers
AssigneeEmery Industries, Inc.
InventorEugene G. Harris
Life of this patent
Estimating the term…
Abstract
Ethylene glycol monoaryl ethers useful as fragrance chemicals and substantially free of undesirable metallic notes are obtained by treating the product with an alkali metal borohydride at a temperature from ambient up to about 100.degree. C.
Claims6
A process for enhancing the fragrance qualities of ethylene glycol monoaryl ethers obtained by the reaction of phenol with ethylene oxide in an alkaline reaction medium and having the formula ##STR2## wherein R is hydrogen, a C.sub.1-8 alkyl group or C.sub.1-8 alkoxyl group which comprises intimately contacting the ethylene glycol monoaryl ether with 0.01 to 1 weight percent alkali metal borohydride at a temperature up to about 100.degree. C., sparging by subsurfacely introducing and dispersing up to 10 weight percent water into the ethylene glycol monoaryl ether at a temperature of 75.degree. C. to 120.degree. C. and pressure less than 100 mm Hg, and drying the ethylene glycol monoaryl ether to a moisture content less than 1 percent.
Dependencies are inferred from the claim text.