# US 4,398,503 A · Method and apparatus for metering a feed of hydrogen fluoride vapor

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- Number: US 4,398,503 A
- Document ID: US4398503A
- Status: Granted
- Kind: A
- Application number: 06/303,114
- Filed: 1981-09-17
- Granted: 1983-08-16
- Earliest claimed: 1979-07-23
- Assignees: British Nuclear Fuels plc
- Inventors: George M. Gillies
- Web page: https://patentgrep.com/patent/US4398503A

## CPC

- B01J 4/008: {Feed or outlet control devices}
- B01J: CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS

## Abstract

A boiler for vaporizing liquid hydrogen fluoride has a heat transfer surface arranged to be covered increasingly by the liquid as the liquid level rises so that the heat supplied to the boiler can be adjusted to maintain a constant level of liquid in the boiler and thereby equate the feed rate of liquid hydrogen fluoride to that vaporized. Thus by metering and controlling the feed rate of the liquid the feed rate of the vapor can be metered and controlled.

## Claims

### Claim 1

A method of producing a metered feed of hydrogen fluoride vapour comprising the steps of
(a) metering a flow of liquid hydrogen fluoride,
(b) introducing the metered flow continuously into liquid hydrogen fluoride contained in a boiler having a heat transfer surface arranged to be increasingly covered by the liquid hydrogen fluoride as the level of the liquid hydrogen fluoride rises in the boiler,
(c) supplying heat to the heat transfer surface continuously in a manner to effect evaporation of the liquid hydrogen fluoride at a rate determined essentially only by the amount of the heat transfer surface covered by the liquid hydrogen fluoride, the heat being supplied to the heat transfer surface by condensing steam out of contact with the hydrogen fluoride,
(d) controlling the metered flow rate within limits set by the size and location of the heat transfer surface for the automatic balance in equilibrium of the rate of evaporation and the metered flow rate with the heat transfer surface always partially covered, and
(e) removing hydrogen fluoride vapour through an outlet from the boiler substantially continuously at the rate of evaporation.