# US 4,396,570 A · Nylon spin-draw process with steam conditioning

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- Number: US 4,396,570 A
- Document ID: US4396570A
- Status: Granted
- Kind: A
- Application number: 06/259,402
- Filed: 1981-05-01
- Granted: 1983-08-02
- Earliest claimed: 1981-05-01
- Assignees: Allied Corporation
- Inventors: Frank L. Peckinpaugh; Michael K. Westmoreland
- Web page: https://patentgrep.com/patent/US4396570A

## CPC

- D01F 6/60: from polyamides (from polyamino acids or polypeptides D01F6/68)
- D01D 5/08: Melt spinning methods {(D01D5/0023 takes precedence)}
- D01D 5/12: Stretch-spinning methods ({D01D5/098 takes precedence} finishing by stretching D02J1/22)
- D01F: CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01D: MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS

## Abstract

This invention is a continuous process for spinning and drawing polycarbonamide filaments as a continuous running length comprising spinning the filaments Y from the molten polymer through a spinnerette 3 into a quench stack 4 and immediately quenching the freshly spun filaments in a quench stack with a flowing quench medium and immediately applying a yarn finish so that after quenching and applying finish, the surface temperature of the filaments is below the second order transition temperature for the filaments at the ambient conditions, and immediately applying steam in a chamber 15 around the continuous running length of filaments at a temperature at from about 60.degree. C. to 95.degree. C. for periods from about 0.03 to 3 seconds and immediately drawing the filaments; and the apparatus to accomplish that process.

## Claims

### Claim 1

A continuous process for spinning and drawing nylon 6 filaments as a continuous running length comprising
(a) spinning the filaments from the molten polymer through a spinnerette into a quench stack, and immediately
(b) quenching the freshly spun filaments in a quench stack with a flowing quench medium followed by a fog of atomized water and immediately
(c) applying a yarn finish so that after quenching and applying finish the surface temperature of the filaments is below 34.degree. C. and above 25.degree. C. and immediately
(d) applying steam in a chamber around the continuous running length of filaments at a chamber temperature of from about 60.degree. C. to 95.degree. C. for a period of from about 0.03 to about 3 seconds,
(e) drawing the filaments.

### Claim 2 (depends on 1)

The process of claim 1 wherein the quenching medium is air.

### Claim 3 (depends on 1)

The process of claim 1 wherein immediately following applying the yarn finish and before applying steam, the filaments are set at a desired denier by passing over a driven godet roll.

### Claim 4 (depends on 1)

The process of claim 1 wherein the steam is applied for a period of from between about 0.1 to about 2 seconds.

### Claim 5 (depends on 1)

The process of claim 1 wherein the filaments are drawn to a draw ratio of from between about 2.2 to about 4.2.

### Claim 6 (depends on 1)

The process of claim 1 wherein the filaments are textured immediately following drawing.

### Claim 7 (depends on 6)

The process of claim 6 wherein texturing is by use of a jet of heated medium.

### Claim 8 (depends on 6)

The process of claim 6 wherein the jet uses steam to impinge the filaments upon a moving screen in a cavity.

### Claim 9 (depends on 1)

The process of claim 1 wherein the quenching medium is a cross-flow of air the filament is set at a desired denier by passing over a driven godet roll, the steam is applied at a chamber temperature of from between about 60.degree. and about 90.degree. C. for a period of from about 0.1 to 2 seconds, the drawing takes place in two stages between sets of driven rolls, the first stage draw ratio being between 1.1 and about 1.2, the second stage draw ratio being between about 2.5 and about 3, the filaments are textured after drawing with steam jet which impinges the filaments on a moving screen in a cavity, and the continuous running length of filaments are taken up at a speed of between about 2500 and 4000 meters per minute and molten polymer is fed to the spinnerette at a rate of from between about 34 and 48 pounds (15 and about 22 kilograms) per hour.