# US 4,396,395 A · Method and apparatus for contacting particulate coal and a deactivating fluid

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- Number: US 4,396,395 A
- Document ID: US4396395A
- Status: Granted
- Kind: A
- Application number: 06/333,144
- Filed: 1981-12-21
- Granted: 1983-08-02
- Earliest claimed: 1981-12-21
- Assignees: Atlantic Richfield Company
- Inventors: James L. Skinner; J. David Matthews
- Web page: https://patentgrep.com/patent/US4396395A

## CPC

- C10F 5/00: Drying or de-watering peat (drying in general F26B)
- C10L 9/10: by using additives
- C10F: DRYING OR WORKING-UP OF PEAT
- C10L: FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G OR C10K; LIQUIFIED PETROLEUM GAS; USE OF ADDITIVES TO FUELS OR FIRES; FIRE-LIGHTERS

## Abstract

A method and apparatus for contacting particulate coal and a deactivating fluid, the apparatus comprising a mist contacting vessel wherein the coal and a deactivating fluid mist are contacted to produce a coal-deactivating fluid mixture. A method for producing the coal-deactivating fluid mixture is disclosed.

## Claims

### Claim 1

An apparatus for intimately contacting a dried low rank coal selected from the group consisting of sub-bituminous, lignite and brown coals with a deactivating fluid to reduce the tendency of said dried low rank coals to spontaneously ignite, said apparatus comprising:
a. a contacting vessel, having a particulate coal inlet and a particulate coal outlet, said particulate coal inlet being positioned so that dried particulate coal charged to said contacting vessel through said particulate coal inlet falls through said contacting vessel to said particulate coal outlet; and,
b. at least one deactivating fluid mist injection means positioned to inject a mist of a deactivating fluid into said contacting vessel between said particulate coal inlet and said particulate coal outlet to intimately contact said particulate coal with said deactivating fluid as said particulate coal falls through said mist of said deactivating fluid.

### Claim 2 (depends on 1)

The apparatus of claim 1 wherein said vessel includes projections positioned on inner walls of said vessel to facilitate intimate contacting of said particulate coal and said mist.

### Claim 3 (depends on 2)

The apparatus of claim 2 wherein said mist injection means comprises at least one tubular member including a plurality of mist nozzles positioned on an inner wall of said vessel.

### Claim 4 (depends on 3)

The apparatus of claim 3 wherein said tubular member is positioned beneath at least one of said projections.

### Claim 5 (depends on 1)

The apparatus of claim 1 wherein at least one deflection means is positioned near said particulate coal outlet to deflect said particulate coal.

### Claim 6 (depends on 5)

The apparatus of claim 5 wherein said mist injection means further comprises at least one tubular member including a plurality of mist nozzles positioned beneath said deflector means.

### Claim 7

A method for intimately contacting a dried low rank coal selected from the group consisting of sub-bituminous, lignite and brown coals with a deactivating fluid to reduce the tendency of said dried low rank coals to spontaneously ignite, said method consisting essentially of:
a. charging said coal to a deactivating fluid mist zone so that said coal falls through said mist zone;
b. maintaining a mist of a deactivating fluid in said mist zone;
c. intimately contacting said coal and said mist to absorb a sufficient quantity of said deactivating fluid onto said coal to produce a deactivated coal as said coal falls through said mist zone; and,
d. recovering said deactivated coal.

### Claim 8 (depends on 7)

The method of claim 7 wherein said coal is charged to said mist zone at a temperature from about 70.degree. to about 110.degree. F.