# US 4,395,310 A · Fractionation system

> Agents: this data is available as JSON from the patentgrep API and MCP server — see https://patentgrep.com/llms.txt

- Number: US 4,395,310 A
- Document ID: US4395310A
- Status: Granted
- Kind: A
- Application number: 06/283,231
- Filed: 1981-07-14
- Granted: 1983-07-26
- Earliest claimed: 1981-07-14
- Assignees: Exxon Research & Engineering Co.
- Inventors: John E. Idenden
- Web page: https://patentgrep.com/patent/US4395310A

## CPC

- B01D 3/322: {Reboiler specifications}
- B01D 3/007: {Energy recuperation; Heat pumps}
- B01D 3/14: Fractional distillation {or use of a fractionation or rectification column}
- C07C 7/04: by distillation
- Y10S 203/04: Heat pump
- Y10S 203/08: Waste heat
- Y10S 203/19: Sidestream
- Y10S 208/01: Automatic control
- B01D: SEPARATION (separating solids from solids by wet methods B03B, B03D; by pneumatic jigs or tables B03B; by other dry methods B07; magnetic or electrostatic separation of solid materials from solid materials or fluids, separation by high-voltage electric fields B03C; centrifuges, vortex apparatus B04; presses per se for squeezing-out liquid from liquid-containing material B30B9/02; treatment of water C02F, e.g. softening by ion-exchange C02F1/42; {arrangements of air intake cleaners in gas turbine plants F02C7/05} ; arrangements or mounting of filters in air-conditioning, air-humidification or ventilation F24F13/28)
- C07C: ACYCLIC OR CARBOCYCLIC COMPOUNDS
- Y10S: TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS

## Abstract

A method for decreasing the external energy input to a fractionation system is disclosed. The method utilizes a compression zone communicating with either the overhead fraction or the bottoms fraction from a fractionation zone. The method is directed at regulating the rate of energy addition and/or removal to the fractionation zone by at least one of the fractions returned to the fractionation zone to maintain the separated fractions within the desired limits.

## Claims

### Claim 1

A method for reducing the energy input to a fractionation system comprising a fractionation zone, a reboiler zone communicating with the fractionation zone, and a compression zone communicating with the fractionation zone and the reboiler zone, said method comprising:
A. introducing a hydrocarbon feed into the fractionation zone, the fractionation zone adapted to separate the feed into an overhead fraction and a bottoms fraction;
B. passing at least a portion of the bottoms fraction from the fractionation zone through a reboiler zone for reheating prior to returning bottoms fraction to the fractionation zone;
C. passing overhead fraction through a compression zone wherein the overhead fraction is compressed;
D. passing substantially all the overhead fraction from the compression zone through the reboiler zone, the compressed overhead fraction transferring heat to the bottoms fraction;
E. returning an overhead fraction consisting of a liquid phase quantity and a vapor phase quantity to the fractionation zone;
F. monitoring the composition of at least one of the fractions separated in the fractionation zone; and,
G. regulating the rate of said liquid phase quantity of the overhead fraction returned to the fractionation zone sufficient to thereby reduce the energy input to the fractionation system as compared to a fractionation system having no compression zone.

### Claim 2 (depends on 1)

The method of claim 1 wherein the overhead fraction from the fractionation zone is preheated prior to entering the compression zone by the overhead fraction from the reboiler zone.

### Claim 3 (depends on 2)

The method of claim 2 wherein at least a portion of the overhead fraction returned to the fractionation zone is further heated by an external heat source.

### Claim 4 (depends on 2)

The method of claim 2 wherein a portion of the overhead fraction from the reboiler zone is removed after preheating the overhead fraction from the fractionation zone.