# US 4,395,296 A · Thermal mechanical process for steel slabs and the product thereof

> Agents: this data is available as JSON from the patentgrep API and MCP server — see https://patentgrep.com/llms.txt

- Number: US 4,395,296 A
- Document ID: US4395296A
- Status: Granted
- Kind: A
- Application number: 06/276,103
- Filed: 1981-06-22
- Granted: 1983-07-26
- Earliest claimed: 1981-06-22
- Assignees: Bethlehem Steel Corporation
- Inventors: Halle Abrams
- Web page: https://patentgrep.com/patent/US4395296A

## CPC

- C21D 8/0226: {Hot rolling}
- C21D 2211/00: Microstructure comprising significant phases
- Y10S 148/902: having portions of differing metallurgical properties or characteristics
- C21D: MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING (surface treatment of metallic material involving at least one process provided for in class C23 and at least one process covered by this subclass C23F17/00; unidirectional solidification of eutectic materials or unidirectional demixing of eutectoid materials C30B)
- Y10S: TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS

## Abstract

This invention is directed to a thermal-mechanical process, and to the product thereof, for treating carbon or low alloy steels to improve their strength and toughness. The process is characterized by the steps of austenitizing a carbon or low alloy steel workpiece, preferably in the form of a slab, reducing said slab at a temperature above about 1900.degree. F. (1038.degree. C.) to a thickness in the range of 2 to 4 inches (5.1 to 10.2 cm), controlled quenching to effect thermal equilibration until a surface-to-center thermal gradient within a temperature range of 50.degree. to 150.degree. F. (28.degree. to 83.degree. C.) is reached, and initiating working such control quenched workpiece at an average temperature within the range of 1450.degree. to 1750.degree. F. (788.degree. to 954.degree. C.). The reduced steel product, having been treated in accordance with said thermal-mechanical process to yield a rolled steel plate having a thickness between about 0.5 to 1.25 inches (1.3 to 3.2 cm), is characterized by a fine-grained microstructure that is essentially grain size symmetrical from the center to the surface, with a grain size difference on the order of about 1 ASTM number, center to sub-surface, and by improved strength and toughness.

## Claims

### Claim 1

In a thermal-mechanical process for treating a carbon or low alloy steel slab by a modified controlled rolling schedule to improve the strength and toughness properties of said steel slab, where such schedule includes a high temperature reduction of the steel slab, and quenching the steel slab to reduce the time for initiating a second low temperature reduction of the steel slab to final thickness, the improvement comprising in combination therewith the steps of
(a) subjecting said steel slab to a high temperature reduction step at a temperature above 2000.degree. F. (1053.degree. C.),
(b) quenching said steel slab from a temperature above about 1900.degree. F. (1038.degree. C.) by the application of low pressure water uniformly to the surfaces thereof, where the rate and time of application of said water is such as to achieve a heat transfer coefficient within the range of 200 to 600 BTU/HR-ft.sup.2 -.degree.F.,
(c) ceasing said quenching prior to the surfaces of said steel slab reaching a temperature of about 1000.degree. F. (539.degree. C.) to avoid transformation of said steel slab to martensite,
(d) holding said steel slab for a period of time to reduce the thermal gradient from surface to center thereof to a range of 50.degree. to 150.degree. F. (28.degree. to 83.degree. C.),
(e) subjecting the steel slab to said second reduction at an average temperature of 1450.degree. to 1750.degree. F. (739.degree. to 954.degree. C.) to form a steel plate, and
(f) cooling said steel plate to ambient temperature, whereby such plate is characterized by a fine-grained microstructure that is essentially grain size symmetrical from the center to the surface of the plate.

### Claim 2 (depends on 1)

The process according to claim 1, characterized by the further improvement that said second reduction is finished at a temperature within the range of 1250.degree. to 1600.degree. F. (677.degree. to 871.degree. C.).

### Claim 3 (depends on 1, 2)

The process according to either one of claims 1 or 2, characterized by the further improvement that the thickness of said steel slab after the high temperature reduction is between about 2 to 4 inches (51 to 102 mm), and the final plate thickness is between about 0.5 to 1.25 inches (13 to 32 mm).

### Claim 4 (depends on 3)

The process according to claim 3 characterized in that the ferrite grain size at the center of said steel plate is about one ASTM number coarser than the ferrite grain size near the plate surface.