# US 4,394,258 A · Froth flotation apparatus with water recovery and method > Agents: this data is available as JSON from the patentgrep API and MCP server — see https://patentgrep.com/llms.txt - Number: US 4,394,258 A - Document ID: US4394258A - Status: Granted - Kind: A - Application number: 06/276,809 - Filed: 1981-06-25 - Granted: 1983-07-19 - Earliest claimed: 1981-06-25 - Assignees: The Diester Concentrator Co., Inc. - Inventors: Donald E. Zipperian - Web page: https://patentgrep.com/patent/US4394258A ## CPC - B03D 1/24: Pneumatic {(mixing gases or vapours with liquids B01F23/20)} - B03D 1/028: {Control and monitoring of flotation processes; computer models therefor} - B03D 1/1431: {Dissolved air flotation machines} - B03D 1/1456: {Feed mechanisms for the slurry} - B03D: FLOTATION; DIFFERENTIAL SEDIMENTATION (sedimentation in general B01D21/00; in combination with other separation of solids B03B; sink-float separation B03B5/28; detergents, soaps C11D) ## Abstract The invention relates to the concentration of particulate matter by froth flotation and in particular to improvements leading to the conservation of water. The apparatus includes an upstanding flotation compartment adapted to contain a relatively quiescent body of aqueous pulp. Aqueous pulp is introduced into and float fraction is collected from the upper portion of the flotation compartment, and hydraulic and aeration compartments are disposed near the bottom of the flotation compartment for aerating the water therein. A water-collecting compartment connected to the bottom of the hydraulic and aeration compartments is adapted to receive water from the latter. A tailings-discharge duct centrally of the flotation compartment extends through the hydraulic, aeration and water collection compartments to discharge fluidized tailings. The water-collecting compartment is connected to drain into a water-replenishing reservoir having an outlet leading to a pump which in turn is connected back to the hydraulic and aeration compartments. The reservoir is adapted to receive other water from a suitable source. Water draining from the water-collecting compartment is thereby recovered and recirculated back to the hydraulic and aeration compartments. ## Claims ### Claim 1 Apparatus for separation of minerals from an aqueous pulp containing a mixture of mineral and gangue particles by froth flotation compising: an upstanding flotation compartment adapted to contain a relatively quiescent body of aqueous pulp, feed means for introducing aqueous pulp into said flotation compartment, froth-collecting means disposed adjacent to the upper end of said flotation compartment for collecting a float fraction of said aqueous pulp, aeration means for applying aerated water to said flotation compartment near the bottom whereby bubbles of air are introduced throughout substantially the entire cross-section of said flotation compartment, said aeration means including a constriction plate substantially spanning said flotation compartment, said constriction plate having a plurality of bubble-receiving apertures spaced throughout the area thereof, tailing-discharge means for discharging an aqueous non-float fraction of unfloated particles of said aqueous pulp from said flotation compartment, water-collecting means below said constriction plate for receiving water from said aeration means, means for inhibiting passage of said non-float fraction from said flotation compartment to said water-collecting means, and pump means for pumping water from said water-collection means back to said aeration means, whereby the water that is collected is recirculated and aerated for application to said flotation compartment. ### Claim 2 (depends on 1) The apparatus of claim 1 including water supply means for replenishing water to said flotation compartment in an amount corresponding to the amount of water discharge from said flotation compartment which includes the discharge from said tailing-discharge means. ### Claim 3 (depends on 1) The apparatus of claim 1 wherein said water-collecting means includes a collecting compartment communicating with said aeration means, and said tailing-discharge means including a duct communicating with said flotation compartment above said aeration means and by-passing said collecting compartment. ### Claim 4 (depends on 3) The apparatus of claim 3 wherein said duct is centrally located with respect to said flotation compartment and extends through said collecting compartment. ### Claim 5 (depends on 3) The apparatus of claim 3 including valve means for controlling the flow of water from said collecting compartment to said pump means. ### Claim 6 (depends on 3) The apparatus of claim 3 wherein said aeration means includes a hydraulic compartment having said constriction plate, said hydraulic compartment having a second apertured plate spanning said flotation compartment spaced below said constriction plate. ### Claim 7 (depends on 6) The apparatus of claim 6 wherein said duct is centrally located with respect to said flotation compartment and extends through said hydraulic and collecting compartments. ### Claim 8 Apparatus for separation of minerals from an aqueous pulp containing a mixture of mineral and gangue particles by froth flotation comprising: an upstanding flotation compartment adapted to contain a relatively quiescent body of aqueous pulp, feed means for introducing aqueous pulp into said floations compartment, froth-collecting means disposed adjacent to the upper end of said flotation compartment for collecting a float fraction of said aqueous pulp, aeration means for applying aerated water to said flotation compartment near the bottom whereby bubbles of air are introduced throughout substantially the entire cross-section of said flotation compartment, tailing-discharge means for discharging an aqueous non-float fraction of unfloated particles of said aqueous pulp from said flotation compartment, water-collecting means for receiving water from said aeration means, means for inhibiting passage of non-float fraction from said flotation compartment to said water-collecting means, pump means for pumping water from said water-collecting means back to said aeration means, whereby the water that is collected is recirculated and aerated for application to said flotation compartment, water supply means for replenishing water to said flotation compartment in an amount corresponding to the amount of water discharged therefrom, said water-collecting means including a water compartment beneath and communicating with said aeration means, and said tailing-discharge means including a duct communicating with said flotation compartment above said aeration means and bypassing said water compartment, said water replenishing means further including a reservoir and a hydraulic line leading thereto from said water compartment, said reservoir having an outlet, and said pump means being connected between said outlet and said aeration means. ### Claim 9 (depends on 8) The apparatus of claim 8 including an adjustable control valve in said hydraulic line for controlling the flow of water therethrough. ### Claim 10 (depends on 9) The apparatus of claim 9 wherein said water-replenishing means includes a source of water in feeding relation to said reservoir, a water level-controlling device in said reservoir, a second control valve in series between said source and said reservoir, means interconnecting said water level-controlling device and said second valve for feeding water to said reservoir upon actuation of said level-controlling device. ### Claim 11 (depends on 10) The apparatus of claim 10 wherein said level-controlling device includes a float, said float being connected to said second valve, said float upon dropping to a first predetermined level causing said second valve to open and upon rising to a second predetermined level causing said second valve to close. ### Claim 12 Apparatus for separation of minerals from an aqueous pulp containing a mixture of mineral and gangue particles by froth flotation comprising: an upstanding flotation compartment adapted to contain a relatively quiescent body of aqueous pulp, feed means for introducing aqueous pulp into said flotation compartment, froth-collecting means disposed adjacent to the upper end of said flotation compartment for collecting a float fraction of said aqueous pulp, hydraulic means for applying water to said flotation compartment near the bottom thereof, aeration means for applying aerated water to said flotation compartment near the bottom whereby bubbles of air are introduced throughout substantially the entire cross-section thereof, tailing-discharge means for discharging an aqueous non-float fraction of unfloated particles of said aqueous pulp past said aeration means and hydraulic means, and means for adjusting the balance of water and aerated water volumes applied by said hydraulic and aeration means. ### Claim 13 (depends on 12) The apparatus of claim 12 wherein said hydraulic means includes a hydraulic compartment separated from the bottom of said flotation compartment by means of an apertured constriction plate. ### Claim 14 (depends on 13) The apparatus of claim 13 wherein said aeration means includes an aeration compartment beneath said hydraulic compartment. ### Claim 15 (depends on 14) The apparatus of claim 14 wherein said aeration compartment is separated from said hydraulic compartment by means of a second apertured constriction plate. ### Claim 16 (depends on 15) The apparatus of claim 15 wherein said hydraulic and aeration means include pipe sections in each of said hydraulic and aeration compartments and a source of water, said adjusting means including individually adjustable valves in series between said source and said pipe sections, respectively. ### Claim 17 (depends on 16) The apparatus of claim 16 including water-collecting means for receiving water from said hydraulic and aeration compartments, and pump means for pumping water from said water-collection means back to said source, whereby the water that is collected is recirculated back to said hydraulic and aeration compartments. ### Claim 18 (depends on 17) The apparatus of claim 17 including water supply means for replenishing water to said flotation compartment in an amount corresponding to the amount of water discharged from said tailing-discharge means, said water-collecting means including a water compartment beneath and communicating with said aeration means, and said tailing-discharge means including a duct communicating with said flotation compartment above said aeration means and bypassing said water compartment, said water-replenishing means further including a reservoir and a hydraulic line leading thereto from said water compartment, said reservoir having an outlet, and said pump means being connected between said outlet and said source. ### Claim 19 (depends on 12) The apparatus of claim 12 wherein said hydraulic and aeration means includes pipe sections extending into a space beneath and in communication with said flotation compartment, and said adjusting means including at least one controllable valve in series with one or more of said pipe sections. ### Claim 20 (depends on 19) The apparatus of claim 19 wherein said hydraulic and aeration means include water source means for supplying pressurized water to said pipe sections, said valve being connected to said source means. ### Claim 21 (depends on 20) The apparatus of claim 20 wherein said source means includes a manifold, said pipe sections being connected to said manifold and having control valves in series therewith, respectively. ### Claim 22 The method of separating minerals from an aqueous pulp containing a mixture of mineral and gangue particles by froth flotation comprising the steps of providing a quantity of water within a compartment, feeding aqueous pulp containing a mixture of water and particles to be connected into the upper region of said compartment, discharging a mixture of water and non-float fraction of said pulp from the lower region of said compartment, controlling the rate of discharge to correspond to the rate of water as contained in the aqueous pulp fed to said compartment, supplying aerated water to the lower region of said compartment for providing a supply of levitating air bubbles and froth for floating the float fraction of said aqueous pulp, collecting froth containing float fraction from the water in said compartment, collecting water from said compartment from a location beneath that at which aerated water is supplied, introducing a hydraulic seal at a location above that at which said water is collected for inhibiting non-float fraction for being included in said collected water, recirculating said collected water to said compartment, and aerating at least a portion of such recirculated water. ### Claim 23 (depends on 22) The method of claim 22 wherein said step of controlling discharge further includes maintaining the water in said compartment at a predetermined level. ### Claim 24 (depends on 23) The method of claim 23 including the step of adding water from an external source to said compartment by introducing it along with said recirculated water. ### Claim 25 (depends on 23) The method of claim 23 including discharging said mixture of water and non-float fraction from a position above that at which aerated water is so supplied. ### Claim 26 Apparatus for separation of minerals from an aqueous pulp containing a mixture of mineral and gangue particles by froth flotation comprising: an upstanding flotation compartment adapted to contain a relatively quiescent body of aqueous pulp, feeding means for introducing aqueous pulp into said flotation compartment, froth-collecting means disposed adjacent to the upper end of said flotation compartment for collecting a float fraction of said aqueous pulp, aeration means for applying aerated water to said flotation compartment near the bottom whereby bubbles of air are introduced throughout substantially the entire cross-section thereof, tailing-discharge means for discharging an aqueous non-float fraction of unfloated particles of said aqueous pulp past said aeration means, means for collecting water from said flotation compartment at a location beneath said aeration means and recirculating it back to said flotation compartment, and means supplying non-aerated water to said aeration means and to the bottom portion of said flotation compartment for inhibiting the gravitating passage therethrough and to said water-collecting means of aqueous non-float fraction. ### Claim 27 (depends on 26) The apparatus of claim 26 wherein said aeration means includes two vertically spaced apertured plates spanning said flotation compartment and means for introducing aerated water therebeneath whereby bubbles levitate through the apertures in said plate, and said non-aerated water supply means including first means for introducing said non-aerated water into the space between said plates. ### Claim 28 (depends on 27) The apparatus of claim 27 including second means for introducing additional non-aerated water beneath said plates. ### Claim 29 (depends on 28) The apparatus of claim 28 including means for replenishing water to said flotation compartment as lost therefrom by adding it to said recirculating means. ### Claim 30 (depends on 29) The apparatus of claim 29 including means for adjusting the rate of flow of aerated and non-aerated water into said flotation compartment, to and between said plates. ### Claim 31 (depends on 28) The apparatus of claim 28 wherein the apertures in the lower of said plates are larger than the apertures in the upper thereof and the non-aerated water admitted to the space therebetween is in such quantity to serve as a hydraulic seal against aqueous non-float fraction from passing to said water-collecting means.