# US 4,394,216 A · Vapor condensate return means in a vapor generating and recovery apparatus

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- Number: US 4,394,216 A
- Document ID: US4394216A
- Status: Granted
- Kind: A
- Application number: 06/334,169
- Filed: 1981-12-24
- Granted: 1983-07-19
- Earliest claimed: 1981-12-24
- Inventors: James W. McCord
- Web page: https://patentgrep.com/patent/US4394216A

## CPC

- B01D 3/00: Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping ({evaporation in general, e.g. of liquids for gas phase reactions B01B1/005;} gas chromatography B01D15/08; destructive distillation C10B; preparation of alcoholic beverages by distillation C12H6/02)
- C23G 5/04: Apparatus
- B01D: SEPARATION (separating solids from solids by wet methods B03B, B03D; by pneumatic jigs or tables B03B; by other dry methods B07; magnetic or electrostatic separation of solid materials from solid materials or fluids, separation by high-voltage electric fields B03C; centrifuges, vortex apparatus B04; presses per se for squeezing-out liquid from liquid-containing material B30B9/02; treatment of water C02F, e.g. softening by ion-exchange C02F1/42; {arrangements of air intake cleaners in gas turbine plants F02C7/05} ; arrangements or mounting of filters in air-conditioning, air-humidification or ventilation F24F13/28)
- C23G: CLEANING OR DE-GREASING OF METALLIC MATERIAL BY CHEMICAL METHODS OTHER THAN ELECTROLYSIS

## Abstract

An apparatus and method for recovering two immiscible fluids in a vapor generating and recovery apparatus wherein water, an immiscible cleaning solvent, and an emuslifying agent are subjected to sufficient heat in a first chamber to vaporize the water and the immiscible solvent and then condense in a second chamber the water and immiscible solvent, returning in separate streams the water and solvent to the first chamber.

## Claims

### Claim 1

A vapor generating and recovery apparatus comprising:
a housing having a vaporizing chamber and a condensing chamber therein separated by a first weir of preselected height;
means to add heat to said vaporizing chamber and means to remove heat from said condensing chamber; and,
means to transfer condensate from said condensing chamber, to said vaporizing chamber, said means to transfer condensate including means to separate components within the condensate and return said separated components in separate streams to said vaporizing chamber, said means to remove heat being disposed within said condensing chamber below the upper extremity of said weir and spaced sufficiently above said means to transfer condensate for providing a constant vapor blanket over the means to remove heat from the condensing chamber.

### Claim 2 (depends on 1)

The apparatus of claim 1 wherein said means to separate components includes a first fluid transfer means having an inlet in said condensing chamber and an outlet in said vaporizing chamber, the outlet being above said inlet and the liquid level in the vaporizing chamber and below the upper extremity of said first weir, said means to separate components further including a second fluid transfer means having an inlet and outlet at or above the outlet of the first heat transfer means and below the upper extremity of the first weir.

### Claim 3 (depends on 2)

The apparatus of claim 2 wherein said first fluid transfer means is a conduit and said second fluid transfer means is a conduit.

### Claim 4 (depends on 2)

The apparatus of claim 2 wherein the vaporizing chamber includes a first and second sub-chamber and the sub-chambers are separated by a second weir of preselected height.

### Claim 5 (depends on 4)

The apparatus of claim 4 wherein the outlet of one of said fluid transfer means is in one sub-chamber and the outlet of the other said fluid transfer means is in the other sub-chamber.

### Claim 6 (depends on 4)

The apparatus of claim 4 wherein the second sub-chamber is provided with ultrasonic vibrating means mounted therein and the outlet of said first fluid transfer means is in flow communication with said second sub-chamber and the outlet of said second fluid transfer means is in flow communication with said first sub-chamber.

### Claim 7 (depends on 6)

The apparatus of claim 6 wherein the first weir separates the condensing chamber from the second sub-chamber and the second sub-chamber is provided with heat means mounted along the wall of said first weir.

### Claim 8 (depends on 1)

The apparatus of claim 1 wherein the means to add heat is a heating device disposed along the bottom of said vaporizing chamber.

### Claim 9

A vapor generating and recovery apparatus comprising:
a housing having a vaporizing chamber sub-divided into a plurality of sub-chambers by weirs of preselected height, and a condensing chamber separated from said vaporizing chamber by a first weir of a preselected height greater than that of any said weirs sub-dividing said vaporizing chamber;
means to add heat to at least one of said sub-chambers of said vaporizing chamber, and means to remove heat from said condensing chamber;
means to transfer condensate from said condensing chamber to at least one of said vaporizing sub-chambers, said transfer means including means to separate components within the condensate and in returning at least one of said separated components to at least one of said vaporizing sub-chambers, said means to remove heat being disposed within said condensing chamber below the upper extremity of said weir.

### Claim 10 (depends on 9)

The apparatus of claim 9 wherein said means to separate components includes a first fluid transfer means having an inlet in said condensing chamber and an outlet in one of said sub-chambers, the outlet being above said inlet and the liquid level in said one of said sub-chambers and below the upper extremity of said first weir, said means to separate components further including a second fluid transfer means having an inlet and outlet at or above the outlet of the first heat transfer means and below the upper extremity of the first weir.

### Claim 11 (depends on 10)

The apparatus of claim 10, wherein said means to add heat includes means to add heat to one of said sub-chambers at a weir dividing it from the other sub-chambers whereby upon addition of heat to a solution in said sub-chamber a temperature differential across said sub-chamber is created.

### Claim 12 (depends on 10)

The apparatus of claim 10 wherein said means to transfer condensate from one of said sub-chambers to another of said sub-chambers further includes pump means for transferring a solution under pressure.
