# US 4,394,176 A · Method of producing silicate-containing granulates

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- Number: US 4,394,176 A
- Document ID: US4394176A
- Status: Granted
- Kind: A
- Application number: 06/341,046
- Filed: 1982-01-21
- Granted: 1983-07-19
- Earliest claimed: 1982-01-21
- Assignees: Aarding Weerstandlas B.V.
- Inventors: Hendrik Loggers
- Web page: https://patentgrep.com/patent/US4394176A

## CPC

- C04B 18/021: {agglomerated by a mineral binder, e.g. cement}
- C04B: LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE {(roofing granules E04D7/005)}; CERAMICS (devitrified glass-ceramics C03C10/00); REFRACTORIES; TREATMENT OF NATURAL STONE

## Abstract

The invention relates to a method of producing silicate-containing granulates having a density of more than 0.7 kg/dm3 and a size of 2 to 40 mm, by mixing sand, a calcium oxide-containing product and water, forming granules and curing same in a moist atmosphere without any substantial condensation of moisture upon the granules to be cured. The granules contain 10 to 14% of moisture and curing is effected at temperatures above 90.degree. C. The granules may contain a filler, such as fly ash.

## Claims

### Claim 1

A method of producing calcium silicate-containing granulates by mixing a calcium oxide bound-containing product with a silicon-containing product, water and, if desired, a filler, subsequently forming granulates from said mixture by means of a heating treatment, while maintaining said granulates in a heated vapour atmosphere, wherein said heated vapour atmosphere is formed by having a heating fluid chosen from moist and non-moist heating fluids acting indirectly upon the granulates in such a way that any direct moisture condensation from the heating fluid upon the granulates is prevented.

### Claim 2 (depends on 1)

The method of claim 1, wherein the moist granulates are disposed in a closed space and indirectly heated, due to the action of a moist heating fluid upon the outer side of the said closed space.

### Claim 3 (depends on 2)

A method according to claim 2, wherein the moist granulates accomodated in a closed vessel, at least comprising one pressure leveling opening, are disposed in a pressure vessel through which heated steam is passed.

### Claim 4 (depends on 1)

The method of claim 1, wherein the moist granules are disposed in a closed space, indirect heat being fed to said space by means of a non-moist liquid heating fluid.

### Claim 5 (depends on 1)

The method of claim 1, wherein the formed steam emitted from the moist granules during the indirect heat supply, is discharged.

### Claim 6 (depends on 1)

The method of claim 1, wherein the formed steam emitted from the moist granules during the indirect heat supply, is discharged and subsequently condensed, while recuperating the heat present therein.

### Claim 7 (depends on 1)

The method of claim 1, wherein the moist granules to be cured contain less than 25% of moisture.

### Claim 8 (depends on 1)

The method of claim 1, wherein the granules are cured at temperatures from 90.degree. C. to 230.degree. C.

### Claim 9 (depends on 1)

The method of claim 1, wherein the granules have a size comprised between 2 and 40 mm diameter.