# US 4,393,700 A · Process and test specimen for determining the adhesion to glass of interlayers for laminated glass by the tensile shear test

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- Number: US 4,393,700 A
- Document ID: US4393700A
- Status: Granted
- Kind: A
- Application number: 06/310,072
- Filed: 1981-10-09
- Granted: 1983-07-19
- Earliest claimed: 1980-10-11
- Assignees: Hoechst Aktiengesellschaft
- Inventors: Klaus Fabian
- Web page: https://patentgrep.com/patent/US4393700A

## CPC

- B32B 17/10761: {containing vinyl acetal}
- B32B 17/10036: {comprising two outer glass sheets}
- G01N 3/24: by applying steady shearing forces (G01N3/26, G01N3/28 take precedence)
- G01N 19/04: Measuring adhesive force between materials, e.g. of sealing tape, of coating
- G01N 33/386: {Glass}
- B32B: LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- G01N: INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES (measuring or testing apparatus or processes other than immunoassay, involving enzymes or microorganisms C12M, C12Q)

## Abstract

Glass laminates used as safety glass consist of several sheets of glass united by adhesive interlayers. The bond strength of such interlayers may be determined in simple manner using a special test specimen by the tensile shear test. The test specimen is parallelipiped-like and the individual sheets thereof are divided each to form an obtuse fracture, the fractures facing the interlayer being staggered. The minimum force required for detaching the interlayer from the individual sheets of the glass laminate is taken as a measure for the bond strength.

## Claims

### Claim 1

A process for determining the adhesion to glass of interlayers for laminated glass by the tensile shear test, which comprises subjecting to a tensile strain a substantially parallelepiped-like test specimen consisting of laminated glass, the individual sheets of glass of which are divided to form an obtuse fracture, the edges of the fractures facing the interlayer being staggered, and determining the minimum force required to detach the interlayer from the individual sheets of the glass laminate.

### Claim 2 (depends on 1)

The process of claim 1, which comprises effecting the tensile strain transversely to the fractures, which latter are arranged parallel to one another and vertically to the longitudinal axis of the test specimen.

### Claim 3 (depends on 1)

The process of claim 1, which comprises employing a test specimen consisting of two rectangular sheets of glass of from 30 to 100 mm length each, of from 5 to 25 mm width each and of from 3 to 10 mm thickness each, which are superposed congruently and united by an interlayer, each sheets being divided to form an obtuse fracture and the fractures being arranged vertically to the longitudinal direction of the test specimen and parallel to one another, and a measuring apparatus appropriate for determining the tensile shear strength.

### Claim 4

A test specimen for determining the adhesion to glass of interlayers for laminated glass by the tensile shear test, consisting of two rectangular sheets of glass of from 50 to 100 mm length each, of from 5 to 25 mm width each and of from 3 to 10 mm thickness each, said sheets being divided to form an obtuse fracture each and said fractures being arranged vertically to the longitudinal direction of the test specimen and parallel to one another and staggered by a certain distance.