# US 4,393,512 A · Hyper-filter-fluorescer spectrometer for x-rays above 120 keV > Agents: this data is available as JSON from the patentgrep API and MCP server — see https://patentgrep.com/llms.txt - Number: US 4,393,512 A - Document ID: US4393512A - Status: Granted - Kind: A - Application number: 06/281,141 - Filed: 1981-07-07 - Granted: 1983-07-12 - Earliest claimed: 1981-07-07 - Assignees: The United States of America as represented by the United States Department of Energy - Inventors: Ching L. Wang - Web page: https://patentgrep.com/patent/US4393512A ## CPC - G01T 1/36: Measuring spectral distribution of X-rays or of nuclear radiation {spectrometry (pulse selection circuits per se H03K; investigation of materials by radiation diffraction G01N23/20; spectrometer tubes H01J49/00)} - G01N 23/223: by irradiating the sample with X-rays or gamma-rays and by measuring X-ray fluorescence - G01N 2223/076: X-ray fluorescence - G01T: MEASUREMENT OF NUCLEAR OR X-RADIATION (radiation analysis of materials, mass spectrometry G01N23/00; tubes for determining the presence, intensity, density or energy of radiation or particles H01J47/00) - G01N: INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES (measuring or testing apparatus or processes other than immunoassay, involving enzymes or microorganisms C12M, C12Q) ## Abstract An apparatus utilizing filter-fluorescer combinations is provided to measure short bursts of high fluence x-rays above 120 keV energy, where there are no practical absorption edges available for conventional filter-fluorescer techniques. The absorption edge of the prefilter is chosen to be less than that of the fluorescer, i.e., E.sub.PRF <E.sub.F, contrary to the prior art technique E.sub.PRF >E.sub.F. In this way, the response function is virtually zero between E.sub.PRF and E.sub.F and well defined and enhanced in an energy band of less than 1000 keV above the 120 keV energy. ## Claims ### Claim 1 In a spectrometer system to provide measurements of x-rays, wherein these x-rays emitted from a source are transmitted through a pre-filter, directed by a first collimator to a fluorescer, re-emitted from the fluorescer as K-fluorescence lines toward a post-filter and directed again by a second collimator to an x-ray detector, the improvement which comprises: said pre-filter for transmitting x-rays, having a predetermined absorption edge; said post-filter for transmitting x-rays to said detector, having a predetermined absorption edge which is more than the absorption edge of said pre-filter; and said fluorescer for emitting K-fluorescence lines toward said post-filter, having a predetermined absorption edge substantially equal to the absorption edge of said post-filter. ### Claim 2 (depends on 1) The improvement of claim 1, wherein the absorption edges of said pre-filter, post-filter and fluorescer are predetermined to eliminate undesirable transmission in the energy band between said fluorescer and pre-filter absorption edges. ### Claim 3 (depends on 2) The improvement of claim 2, wherein the adjustment of said energy band by preselecting the thickness and material of said pre-filter, post-filter and fluorescer, eliminates the detection by said detector of the gold K-lines emitted when measuring x-rays from a gold target. ### Claim 4 (depends on 1) The improvement of claim 1, wherein the thickness and material of said pre-filter, post-filter and fluorescer are preselected to adjust the response function peak position of said spectrometer system. ### Claim 5 (depends on 1) The improvement of claim 1, wherein said absorption edges are predetermined to provide x-ray measurements in an energy band of less than 1000 keV above 120 keV energy. ### Claim 6 (depends on 1) The improvement of claim 1, wherein said post-filter thickness and material is preselected to improve the signal-to-noise ratio by transmitting the K-fluorescence lines of said x-rays and absorbing the fluorescence or background x-rays. ### Claim 7 A method for measuring x-rays above 120 keV energy, in a spectrometer system comprising a pre-filter, two collimators, a fluorescer, a post-filter and a detector, including the steps of: transmitting said x-rays by said pre-filter having a predetermined absorption edge; transmitting said x-rays to said detector by said post-filter having a predetermined absorption edge which is more than the absorption edge of said pre-filter; re-emitting said x-rays as K-fluorescence lines toward said post-filter, by a fluorescer having a predetermined absorption edge equal to the absorption edge of said post-filter. ### Claim 8 (depends on 7) The method of claim 7, which further comprises the steps of: adjusting the response function peak position of said spectrometer system for a desired energy band by preselecting the thickness and material of said post-filter, pre-filter and fluorescer; adjusting said energy band in less than 1000 keV for x-ray measurements above 120 keV, by preselecting said absorption edges. ### Claim 9 (depends on 7) The method of claim 7, which further comprises the step of: adjusting the energy band between said fluorescer and pre-filter absorption edges of said spectrometer system in order to eliminate the detection by said detector of the gold K-lines when measuring x-rays from a gold source.