# US 4,391,931 A · Capsules containing self-setting compositions and the compositions

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- Number: US 4,391,931 A
- Document ID: US4391931A
- Status: Granted
- Kind: A
- Application number: 06/291,852
- Filed: 1981-08-10
- Granted: 1983-07-05
- Earliest claimed: 1981-08-10
- Inventors: Jeffrey G. Haigh; Leslie W. Cheriton
- Web page: https://patentgrep.com/patent/US4391931A

## CPC

- C08K 3/20: Oxides; Hydroxides {(graphene oxides C08K3/042)}
- C08J 3/241: {Preventing premature crosslinking by physical separation of components, e.g. encapsulation}
- C08K 3/22: of metals
- C08K: Use of inorganic or non-macromolecular organic substances as compounding ingredients (paints, inks, varnishes, dyes, polishes, adhesives C09)
- C08J: WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H (working, e.g. shaping, of plastics B29)

## Abstract

Water and a hydrated salt are both present to reduce the flammability of a flammable resin system, e.g. a capsule having two compartments each containing an interactive component and for use in e.g. a mine.

## Claims

### Claim 1

A capsule containing in separate compartments the interactive components of a self-setting composition, one component comprising an unhardened resin and the other component comprising a hardener therefor, the capsule being rupturable to release the interactive components to intermix them and form the self-setting composition, at least one of the components beig flammable, both free water and hydrated salt being present, the free water or the hydrated salt or both being located in at least one of the components prior to the interaction thereof, the concentration of the free water and the hydrated salt being sufficient to supress the flame of the flammable component but still permitting the set composition to have a strength which exceeds 20 Newtons/mm.sup.2.

### Claim 2 (depends on 1)

A capsule according to claim 1, characterised in that the hydrated salt is one which releases water at a temperature below 150.degree. C.

### Claim 3 (depends on 2)

A capsule according to claim 2, characterised in that the hydrated salt is one which releases water at a temperature below 40.degree. C.

### Claim 4 (depends on 1)

A capsule according to claim 1, characterised in that the hydrated salt is selected from aluminium sulphate, sodium aluminium sulphate, potassium aluminium sulphate, sodium sulphate, gypsum and copper sulphate.

### Claim 5 (depends on 1)

A capsule according to claim 1, characterised in that the hydrated salt is present in one or each of the interactive components in a concentration of from 10% to 50% by weight of the component.

### Claim 6 (depends on 1)

A capsule according to claim 1, characterised in that free water is present in one or each of the interactive components in a concentration of below the level at which it will substantially weaken the strength of the set composition or substantially affect the viscosity thereof.

### Claim 7 (depends on 6)

A capsule according to claim 6, characterised in that one or each interactive component includes a filler selected from ground firebrick or limestone, sand or the like and the free water is absorbed into the filler.

### Claim 8 (depends on 6, 7)

A capsule according to claim 6 or 7, characterised in that the viscosity of the component is about 5000 poise at 20.degree. C. when measured on a Brookfield RVF Helipath Viscometer.

### Claim 9 (depends on 1)

A capsule according to claim 1, characterised in that the concentration of water is sufficient to extinguish flame within 5 seconds.

### Claim 10 (depends on 1)

A capsule according to claim 1, characterised by the presence of a film forming ingredient to seal drops of burning flammable material.

### Claim 11 (depends on 10)

A capsule according to claim 10, characterised in that the film forming ingredient is a wax.

### Claim 12

A self-setting composition comprising first and second components, the first component comprising an unhardened resin and the second component comprising a hardener therefor, the two components being intermixed to form said self-setting composition, at least one of the components being flammable, both free water and hydrated salt being present, the free water or the hydrated salt or both being associated with at least one of the components prior to intermixing, the concentration of the free water and the hydrated salt being sufficient to suppress the flame of the flammable component but still permitting the set composition to have a strength which exceeds 20 Newtons/mm.sup.2.

### Claim 13 (depends on 12)

A composition according to claim 12, characterised in that the hydrated salt is present in one dry interactive component.