# US 4,391,608 A · Process for the beneficiation of carbonous materials with the aid of ultrasound

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- Number: US 4,391,608 A
- Document ID: US4391608A
- Status: Granted
- Kind: A
- Application number: 06/289,536
- Filed: 1981-08-03
- Granted: 1983-07-05
- Earliest claimed: 1980-03-31
- Inventors: Michael A. Dondelewski
- Web page: https://patentgrep.com/patent/US4391608A

## CPC

- C10L 9/00: Treating solid fuels to improve their combustion
- Y10S 44/904: Method involving electric or wave energy
- C10L: FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G OR C10K; LIQUIFIED PETROLEUM GAS; USE OF ADDITIVES TO FUELS OR FIRES; FIRE-LIGHTERS
- Y10S: TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS

## Abstract

A process for reducing the sulfur and ash content of coal and the like by treatment in an aqueous slurry with ultrasound followed by subsequent separating steps.

## Claims

### Claim 1

A method of treating coal to reduce ash and sulfur content comprising the steps for:
(a) combining the coal with water and oil to form a slurry, said oil being a semi-reactive oil containing esters of fatty acids,
(b) applying ultrasound to said slurry to cause separation of ash from coal and sulfur including organic sulfur from coal,
(c) physically separating coal and adhered oil from the slurry and washing to separate ash and sulfur from the coal to recover coal with reduced sulfur and ash content.

### Claim 2 (depends on 1)

A method according to claim 1 wherein the coal is first crushed and sized to a more or less uniform dimension.

### Claim 3 (depends on 1)

A method according to claim 1 wherein said oil is present in an amount up to 5% by weight of the coal added to the slurry.

### Claim 4 (depends on 1, 2)

A method according to claims 1 or 2 wherein sodium chloride is added to the slurry.

### Claim 5 (depends on 1, 2)

A method according to claims 1 or 2 wherein the frequency of applied sound is between 20 and 40 kilocycles per second.

### Claim 6 (depends on 1, 2)

A method according to claims 1 or 2 wherein the temperature of the slurry is maintained less than 75.degree. C.

### Claim 7 (depends on 1, 2)

The method according to claims 1 or 2 wherein the weight ratio of coal to water in the slurry comprises between about 1:20 and 1:3.