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US 4,380,592 AGranted
Process for the production of polyhydroxy lignin-cellulose silicate polymer
OwnerDavid H. Blountinventor
Life of this patent
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Abstract
An alkali metal broken-down plant silicate polymer is reacted with a Lewis acid and an epoxide compound to produce a polyhydroxy lignin-cellulose polymer which may be reacted with polyisocyanates to prodice polyurethane silicate foam and be used for insulation.
Claims24
The process for the production of foamed polyurethane silicate products by the following steps:
- (a) mixing and reacting the following components, thereby producing a polyhydroxy lignin-cellulose polymer;
- (i) a broken-down alkali metal plant silicate polymer produced by heating a mixture of 3 parts by weight of a cellulose-containing plant and 1 to 2 parts by weight of an oxidated silicon compound with 3 to 5 parts by weight of a melted alkali metal hydroxide to between 150.degree. C. and 220.degree. C. while agitating for 5 to 60 minutes;
- in an amount of 100 parts by weight;
- (ii) an epoxide compound, in an amount of 1 to 3 parts by weight;
- (iii) a Lewis acid, in an amount wherein the pH of the mixture of components (i), (ii) and (iii) is 5 to 6:
- (b) mixing and reacting 100 parts by weight of the polyhydroxy lignin-cellulose silicate polymer as produced in step (a), 1 to 600 parts by weight of a compound containing at least two isocyanate groups up to 50% by weight of an inert blowing agent, percentage based on the weight of the reaction mixture.
3 more elements
Dependencies are inferred from the claim text.