Method for drying polyolefins
AssigneeSumitomo Chemical Company, Limited
InventorsShinichi Saito, Kazuo Aikawa, Michio Orino, Kazuya Aoi, Hideo Kusakabe
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Abstract
Method for drying poly(.alpha.-olefins) comprising contacting poly(.alpha.-olefins) having a content of hydrocarbon medium of 0.2 to 2% by weight with nitrogen gas having substantially no hydrocarbon medium and having a dew point of -10.degree. C. or lower in counterflow in a silo type through-flow drying apparatus whereby poly(.alpha.-olefins) having a content of the hydrocarbon medium of less than 0.2% by weight can be obtained.
Claims2
A method for drying a poly(.alpha.-olefin), which comprises supplying nitrogen gas having a dew point of -10.degree. C. or lower into a silo type through-flow drying apparatus from the lower part thereof and contacting a poly(.alpha.-olefin) having a content of hydrocarbon medium of 0.2 to 2% by weight with said nitrogen gas in counterflow in said drying apparatus, the amount of nitrogen gas supplied being 20 to 40 Nm.sup.3 per 1 ton of the poly(.alpha.-olefin), said drying in the silo type through-flow drying apparatus being carried out at a temperature of 70.degree. to 130.degree. C. and a retention time of the poly(.alpha.-olefin) of 0.5 to 20 hours.
In a method for drying poly(.alpha.-olefins), which comprises the steps of subjecting poly(.alpha.-olefins) containing a hydrocarbon medium to centrifugation in order to remove most of the hydrocarbon medium and drying the poly(.alpha.-olefins) thus treated in a drying machine until the content of the hydrocarbon medium comes in the range of 0.2 to 2% by weight, the improvement which comprises supplying nitrogen gas having a dew point of -10.degree. C. or lower into a silo type through-flow drying apparatus from the lower part thereof and contacting said poly(.alpha.-olefin) having a content of hydrocarbon medium of 0.2 to 2% by weight with said nitrogen gas in counterflow in said drying apparatus, the amount of nitrogen gas supplied being 20 to 40 Nm.sup.3 per 1 ton of the poly(.alpha.-olefin), said drying in the silo type through-flow drying apparatus being carried out at a temperature of 70.degree. to 130.degree. C. and a retention time of the poly(.alpha.-olefin) of 0.5 to 20 hours.
Dependencies are inferred from the claim text.