Automatically fed distillation and fractionation system

A distillation system for the separation of liquid mixtures which comprises:

• an inclined still consisting of sidewalls, a lower endwall, an upper endwall, a bottom floor, and a translucent light transmitting top all being joined together to form a sealed still compartment, said compartment being divided into an upper vaporization chamber and a lower preheating chamber by a vaporization floor sealed to said sidewalls and lower endwall parallel to said bottom floor and translucent top, said vaporization floor terminating at its upper end short of said upper endwall, thereby forming a baffle over which liquid from said preheating chamber may overflow into said vaporization chamber, means located on the top surface of said vaporization floor to impede the downward flow of liquid on said surface, means located in said preheating chamber for heating said vaporization floor and liquid contained in the preheating chamber to a specified temperature, inlet means for introducing liquid mixture feed into the lower end of said preheating chamber, outlet means for removing residual liquid from the lower end of said vaporization chamber, and outlet means in said upper endwall for removing vapors formed within the still compartment;
• feed control means interconnected with the inlet means to said preheating chamber for controlling the amount of liquid that flows thereinto, said feed control means consisting of a feed chamber having an inlet and an outlet and a hydraulically operated float control valve, which valve controls the flow of feed liquid through the feed chamber to the preheating chamber, said float control valve being selectively positioned substantially level with said baffle, such that, when liquid in the preheating chamber is below a specified temperature, the valve will remain closed, and when liquid in the preheating chamber is raised to at least said specified temperature, the liquid in the preheating chamber expands in volume, thereby becoming less dense, and is pushed over the baffle end of the vaporization floor by the more dense, cooler liquid feed in the feed chamber that flows by gravity through the outlet of the feed chamber to the preheating chamber, the exiting of liquid feed from the feed chamber causing the float control valve to open, thereby allowing feed liquid to flow through the inlet to the feed chamber as long as the temperature of the feed liquid in the preheating chamber is above the specified temperature and the feed liquid is overflowing the baffle end of the vaporization floor;
• and
• and insulated condensation section interconnected with said still compartment consisting of a fractionation column which receives distilled vapors from the outlet means in the upper endwall of the still compartment, and condenser means for receiving and condensing vapors from the fractionation column into a distillate.