US 4,361,528 A · Method of making thermoplastic dental impression tray

Abstract

A method of making a thermoplastic dental impression tray which can be heated, placed into the patient's mouth where it can be intimately molded to approximate the patient's tissues and characterized in that the tray will maintain its molded structure to a high degree of accuracy. Methyl methacrylate monomer liquid and polymer powder are mixed together and the mixture is allowed to reach a doughy state. The mixture is placed into a mold conforming to the desired structure of the tray. The mold is then heated for a sufficient time under pressure to polymerize the monomer to provide a tray characterized in that when heated to above 135.degree. F. it wil become soft enough so that it can be placed into the patient's mouth for intimate molding therein and which will become so hard when cooled in the mouth that it will exhibit a recovery rate of less than 2% after removal from the mouth so that the precision of the impression is accurately maintained.

Claims15

Dependent claims

A method of making a thermoplastic dental impression tray which is capable of being molded in the mouth of a patient after reheating, said method comprising the steps of:

(a) mixing 45-55% by weight of a methylmethacrylate liquid monomer and 45-55% by weight of a suitable liquid plasticizer to form a plasticized liquid monomer;
(b) mixing said plasticized liquid monomer with methylymethacrylate polymer powder in a ratio of 1:3-3.5 parts by weight to form a mixture;
(c) allowing the mixture to reach a doughy-like state;
(d) placing said mixture into a mold conforming to the desired structure of the tray;
(e) heating the mold at a temperature of about 145.degree.-155.degree. C. for about 4-8 minutes under pressure of about 1,000-2,000 p.s.i. to provide a tray that may be subsequently molded in the patient's mouth after heating it to above about 135.degree. F., with the tray accurately maintaining its molded structure after removal from the mouth;
and
(f) removing the tray from the mold.

4 more elements

A method of making a thermoplastic dental impression tray capable of being molded in the mouth of a patient after reheating, said method comprising the steps:

a. blending not more than about 55% by weight of a non-crosslinked liquid methylmethacrylate monomer with not less than about 45% by weight of suitable liquid plasticizer in a container;
b. placing the container in a cooler at a temperature of about -10.degree. F.;
c. mixing the liquid blend with a methlymethacrylate polymer powder in the ratio of about 3.5 parts by weight polymer powder to one part by weight of the liquid blend;
d. pouring the mixture into a shallow pan;
e. allowing the mixture to reach a doughy-like consistency;
f. cutting the mixture into a plurality of bars weighing between 0.03-0.04 lbs.;
g. placing a bar into a mold made of brass beryllium;
h. heating the mold at a temperature of about 150.degree. C. for about 41/2 minutes at a pressure of about 1,000 psi to sufficiently polymerize the monomer to provide a tray that may be molded in a patient's mouth after heating to above 135.degree. F., with the tray accurately maintaining its molded structure after removal from the mouth characterized by a recovery rate of less than about 2%;
i. cooling the mold at a temperature of about 45.degree.-60.degree. C. at a pressure of about 1000 psi for about 41/2 minutes;
and
j. removing the tray from the mold.

8 more elements

Dependencies are inferred from the claim text.

Method of making thermoplastic dental impression tray

Life of this patent

Method of making thermoplastic dental impression tray

Life of this patent

Abstract

Claims15