Depolymerized cellulosic material with low crystallinity obtained from cellulosic fibers and process for its manufacture
AssigneeBattelle Memorial Institute
InventorsJean-Pierre Sachetto, Jean-Pierre Michel, Sergio Cuccolo, Alain Regnault
Life of this patent
Estimating the term…
Abstract
Depolymerized cellulose powder having substantially an amorphous structure which is obtained by letting cellulose fibers dissolve in concentrated hydrochloric acid of about 40% and at a temperature of at least 38.degree. C. A homogeneous acid hydrolysis is carried out under well controlled conditions in order to depolymerize the dissolved cellulose and is stopped when the cellulose has achieved a mean degree of polymerization between 10 and 200. The depolymerized dissolved cellulose is then separated and processed in order to obtain the aforesaid powder of amorphous depolymerized cellulose.
Claims14
Depolymerized cellulose material having a degree of crystallinity of at least 17% but not exceeding 70%, an average degree of polymerization DP.sub.m corresponding to 10 to 200 units of anhydroglucose and being in powdered form with a low moisture content, the particles of the powdered material being microporous and having a globular shape with rounded angles.
Dependencies are inferred from the claim text.