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US 4,309,371 AGranted
Preparing refractory insulating products having controlled porosity by the wet method
AssigneeGroupement pour les Activities Atomiques et Advancees
InventorsJean Daviot, Michel Marchais
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Abstract
Process for preparing, by the wet method, refractory insulating products, comprising mixing a refractory aluminous cement, a refractory aggregate, and aluminous fibers, making a stable emulsion in water of said mixture, molding and drying the product, and firing the molded product at a temperature lower than its sintering temperature.
Claims7
A process for preparing, by the wet method, non-sintered refractory products of controlled porosity having resistance to molten aluminum, aluminum-base alloys, zinc and zinc-base alloys, comprising the following steps:
- producing a solid mixture of a refractory aluminous cement and a ceramic mixture of:
- a refractory aggregate selected from the group consisting of tabular alumina, corindon, stabilized zirconia and calcium zirconate, and
- refractory ceramic polycrystalline fibers comprising at least 70% by weight alumina and at most 30% silica, the proportion of ceramic fibers being higher than 10% by weight of the amount of refractory aggregate, and the proportion of the ceramic mixture being between 10% and 70% by weight of the total mixture;
- dispersing said solid mixture in water;
- emulsifying the dispersed product by adding 0.5% to 3% by weight, in relation to the weight of the water, of a foaming agent which is stable in a medium of a pH greater than 3;
- stabilizing the emulsion by adding a stabilizing agent;
- molding and drying the product in a mould having lubricated walls;
- and firing the molded product at a temperature higher than 150.degree. C. but lower than its sintering temperature.
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Dependencies are inferred from the claim text.