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US 4,302,576 AGranted
Lactone copolymers as stripping aids in recovery of polymer from solution
AssigneePhillips Petroleum Company
InventorLarry L. Nash
Life of this patent
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Abstract
A process for recovering a rubbery polymer from a rubber-in-solvent solution by steam-stripping the solution to produce rubber crumb in aqueous phase using a low molecular weight lactone copolymer as stripping aid.
Claims8
In a steam-stripping process for recovering a polymer prepared by polymerizing an olefinically unsaturated monomer in a hydrocarbon solvent with an organometal initiator wherein the resulting polymer-in-hydrocarbon solvent solution is steam-stripped to remove said hydrocarbon solvent and to produce polymer crumb in aqueous phase after shortstopping the process of polymerizing.
- the improvement which comprises employing during said steam-stripping an effective steam-stripping amount of a low molecular weight lactone copolymer as stripping aid,
- wherein said lactone copolymer is a copolymer of a lactone with a conjugated diene and/or a monovinylarene, and has a molecular weight of about 2000 to 100000.
Dependencies are inferred from the claim text.