NMR Test method for dispersion of solids in elastomer compositions
AssigneeThe Provost Fellows and Scholars of the College of the Holy and Undivided Trinity of Queen Elizabeth
InventorsGerald E. Wardell, Vincent J. McBrierty
Life of this patent
Estimating the term…
Abstract
An NMR test method is provided for determining the homogeneity of dispersion of a filler substance such as carbon black in an elastomer composition such as a rubber, either on an arbitrary scale or by reference to a standard dispersion of optimum homogeneity which is given the value 1.0 on a linear scale. The method involves measuring the intensity of the short component and the total intensity of the proton free induction decay, of a sample of the dispersion deriving the ratio P.sub.t of said intensities, and optionally deriving a second similar ratio P.sub.s from the standard dispersion to permit a value P.sub.t /P.sub.s on said linear scale to be derived.
Claims7
A method for measuring the homogeneity of a dispersion of a filler substance in an elastomer composition, which method comprises:
- measuring, in an NMR pulse spectrometer, the intensity of a short component and a total intensity, of the proton free induction decay, of a sample of the dispersion under investigation, and deriving the ratio of the short component intensity and the total intensity obtained, said ratio (P.sub.t) representing an empirical measure of the homogeneity of the dispersion under investigation.
Dependencies are inferred from the claim text.