Process for preparing a substantially crystalline sodium aluminosilicate
AssigneeKali-Chemie Aktiengesellschaft
InventorsHelmut Derleth, Ludwig Walter, Karl-Heinrich Bretz, Artur Kurs
Life of this patent
Estimating the term…
Loading patent…
AssigneeKali-Chemie Aktiengesellschaft
InventorsHelmut Derleth, Ludwig Walter, Karl-Heinrich Bretz, Artur Kurs
Estimating the term…
A process for preparing a synthetic substantially crystalline sodium aluminosilicate of the zeolite A type is disclosed. The process comprises rapidly and simultaneously introducing a sodium silicate and a sodium aluminate solution under thorough agitation at a constant by volume ratio which provides for a reaction mixture the content of which is equivalent to a molar ratio of x' Na.sub.2 O/ 1 Al.sub.2 O.sub.3 / y SiO.sub.2 /z' H.sub.2 O wherein x' is from about 6.5 to about 9.0, y is from about 1.7 to about 2.2 and z' is from about 180 to about 250, maintaining the reaction mixture at a temperature of from about 70.degree. to about 100.degree. C. under stirring for a sufficient period of time, usually 1-3 hours, in order to allow the initially amorphous reaction product to crystallize and recovering the substantially crystalline product from the resulting suspension. The essential feature of the process is a continuously maintained constant molar ratio Na.sub.2 O/ Al.sub.2 O/ SiO.sub.2 /H.sub.2 O throughout the reaction mixture during the entire course of the process. The resulting product exhibits a small particle size, an excellent wettability and a high calcium binding power, and is especially suited as a detergent additive.
A process for preparing a synthetic substantially crystalline sodium aluminosilicate of the molar composition xNa.sub.2 O.Al.sub.2 O.sub.3.ySiO.sub.2.zH.sub.2 O, wherein x is a value of from about 0.8 to about 1.2, y is a value from about 1.7 to about 2.2, and z is a value from about 3.0 to about 10.0 which comprises the steps of:
Dependencies are inferred from the claim text.