Porous carbon support materials useful in chromatography and their preparation
AssigneeMerck Patent GmbH
InventorsKlaus Unger, Heinz Gotz
Life of this patent
Estimating the term…
Loading patent…
AssigneeMerck Patent GmbH
InventorsKlaus Unger, Heinz Gotz
Estimating the term…
A process for preparing porous carbon support materials comprises treating activated carbon or coke, having a particle size of about 5 to about 50 .mu.m, a specific surface area of about 10 to 1,000 m.sup.2 /g, a hardness of at least about 95% attrition resistance, with solvent or solvents, and then heat treating the activated carbon or coke at a temperature of about 2,400-3,000.degree. C. under an inert, gas atmosphere; said solvent or solvents affecting the mineral and organic impurities in the activated carbon or coke such that after said subsequent heat treatment, substantially all of said impurities are removed. A hard, mechanically stable, porous carbon support material consisting essentially of highly purified activated carbon, highly purified coke or a mixture thereof, said support material having a carbon content of at least 99%, a specific surface area of about 1 to about 5 m.sup.2 /g and a particle size of about 5 to about 50 .mu.m, may be prepared in this way.
A process for preparing porous carbon support materials useful in chromatography, which comprises treating activated carbon or coke, having a particle size of about 5 to about 50 .mu.m, a specific surface area of about 10 to about 1,000 m.sup.2 /g, and a hardness of at least about 95% attrition resistance, with a solvent or solvents, and then heat treating the activated carbon or coke at a temperature of about 2,400.degree.-3,000.degree. C. under an inert, gas atmosphere;
A hard, mechanically stable, porous carbon support material useful in chromatography consisting essentially of highly purified activated carbon, highly purified coke, or a mixture thereof, said support material having a carbon content of at least 99%, a specific surface area of about 1 to about 5 m.sup.2 /g a particle size of about 5 to about 50 .mu.m and a graphitzed carbon surface.
Dependencies are inferred from the claim text.