Emulsion preparation method using a packed tube emulsifier
AssigneeExxon Research & Engineering Co.
InventorsNorman N. Li, Taras Hucal
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AssigneeExxon Research & Engineering Co.
InventorsNorman N. Li, Taras Hucal
Estimating the term…
Emulsions are prepared utilizing an emulsification device comprising an enclosure having orifices thereby permitting flow of a fluid through the enclosure along one of its axis, of any cross-section profile perpendicular to its axis for fluid flow, which enclosure is packed with a material which causes the flow of fluids to be broken down into many fine streams which fine streams, being in intimate contact one with the other, remix rapidly and repeatedly, resulting in the formation of the desired emulsion. The fluids which are mixed in the packed enclosure are fed to the enclosure by fluid feeding means such as pumps or by gravity feed tanks and conduits communicatively attached to the packed enclosure. The fluids fed into the packed enclosure are introduced into the enclosure in close proximity one to another so as to insure maximum intermixing of the different fluids.
A method for generating emulsions of immiscible fluids, which emulsions have an internal to external phase ratio from 1:1 to greater than 32:1 and a droplet size of from .mu. to greater than 50.mu., which comprises simultaneously passing the immiscible fluids through an enclosure having at least one entrance orifice and at least one exit orifice thereby permitting the flow of said fluids through the enclosure along one of its axis from the entrance to the exit orifice, which enclosure is of any cross-sectional profile perpendicular to the axis of fluid flow, which emclosure is packed with metal sponge which causes the rapid and repeated mixing and remixing of said immiscible fluids in the enclosure and results in the formation of the desired emulsion.
A method for generating emulsions of immiscible fluids, which emulsions have an internal to external phase ratio of from 1:1 to greater than 32:1 and a droplet size of from 1.mu. to greater than 50.mu., which comprises simultaneously passing the immiscible fluids through an enclosure having at least one entrance orifice and at lease one exit orifice thereby permitting the flow of said fluids through the enclosure along one of its axis from the entrance to the exit orifice, which enclosure is of any cross-sectional profile perpendicular to the axis of fluid flow, which enclosure is packed with metal shavings which cause the rapid and repeated mixing and remixing of said immiscible fluids in the enclosure and results in the formation of the desired emulsion.
A method for generating emulsions of immiscible fluids, which emulsions have an internal to external phase ratio of from 1:1 greater than 32:1 and a droplet size of from 1.mu. to greater than 50.mu., which comprises simultaneously passing the immiscible fluids through an enclosure having at least one entrance orifice and at least one exit orifice thereby permitting the flow of said fluids through the enclosure along one of its axis from the entrance to the exit orifice, which enclosure is of any cross-sectional profile perpendicular to the axis of fluid flow, which enclosure is packed with ceramic chips, which causes the rapid and repeated mixing and remixing of said immiscible fluids in the enclosure and results in the formation of the desired emulsion.
A method for generating emulsions of immiscible fluids, which emulsions have an internal to external phase ratio of from 1:1 to greater than 32:1 and a droplet size of from 1.mu. to greater than 50.mu., which comprises simultaneously passing the immiscible fluids through an enclosure having at least one entrance orifice and at least one exit orifice thereby permitting the flow of said fluids through the enclosure along one of its axis from the entrance to the exit orifice, which enclosure is of any cross-sectional profile perpendicular to the axis of fluid flow, which enclosure is packed with Cannon packing which causes the rapid and repeated mixing and remixing of said immiscible fluids in the enclosure and results in the formation of the desired emulsion.
A method for generating emulsions of immiscible fluids, which emulsions have an internal to external phase ratio of from 1:1 to greater than 32:1 and a droplet size of from 1.mu. to greater than 50.mu., which comprises simultaneously passing the immiscible fluids through an enclosure having at least one entrance orifice and at least one exit orifice thereby permitting the flow of said fluids through the enclosure along one of its axis from the entrance to the exit orifice, which enclosure is of any cross-sectional profile perpendicular to the axis of fluid flow, which enclosure is packed with animal hair or plastic brush, which causes the rapid and repeated mixing and remixing of said immiscible fluids in the enclosure and results in the formation of the desired emulsion.
A method for generating emulsions of immiscible fluids, which emulsions have an internal to external phase ratio of from 1:1 to greater than 32:1 and a droplet size of from 1.mu. to greater than 50.mu., which comprises simultaneously passing the immiscible fluids through an enclosure having at least one entrance orifice and at least one exit orifice thereby permitting the flow of said fluids through the enclosure along one of its axis from the entrance to the exit orifice, which enclosure is of any cross-sectional profile perpendicular to the axis of fluid flow, which enclosure is packed with metal tubes shorter than the internal diameter of the enclosure which causes the rapid and repeated mixing and remixing of said immiscible fluids in the enclosure and results in the formation of the desired emulsion.
A method for generating emulsions of immiscible fluids, which emulsions have an internal to external phase ratio of from 1:1 to greater than 32:1 and a droplet size of from 1.mu. to greater than 50.mu., which comprises simultaneously passing the immiscible fluids through an enclosure having at least one entrance orifice and at least one exit orifice thereby permitting the flow of said fluids through the enclosure along one of its axis from the entrance to the exit orifice, which enclosure is of any cross-sectional profile perpendicular to the axis of fluid flow, which enclosure is packed with Berl Saddle, which causes the rapid and repeated mixing and remixing of said immiscible fluids in the enclosure and results in the formation of the desired emulsion.
Dependencies are inferred from the claim text.