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US 4,146,547 AGranted
Manufacture of Bz-1-bromobenzanthrone
AssigneeBASF SE
InventorsAlfred Schuhmacher, Karl-Erich Kling
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Abstract
A process for the manufacture of Bz-1-bromobenzanthrone by brominating finely divided benzanthrone in aqueous suspension, wherein the improvement comprises treating benzanthrone having a mean particle size of 30 .mu.m or less with bromine or brominating agent at above 80.degree. C. A product which contains from 91 to 94% by weight of Bz-1-bromobenzanthrone is obtained.
Claims10
In a process for the manufacture of Bz-1bromobenzanthrone by brominating finely divided benzanthrone with bromine or a brominating agent in aqueous suspension, the improvement which comprises:
- suspending benzanthrone which has a mean particle size of 30 .mu.m or less in a single reaction medium consisting essentially of water;
- heating the suspension to 80.degree. or above;
- and
- then adding said bromine or brominating agent gradually to the suspension maintained at a temperature above 80.degree. C., the molar ratio of the added bromine or brominating agent to benzanthrone being approximately 1:1, thereby resulting in yields of Bz-1-Bromobenzanthrone of at least about 91%.
1 more element
Dependencies are inferred from the claim text.