Coprecipitation process
AssigneeWyrough and Loser, Inc.
InventorsThomas J. Leo, Anders H. Johansson
Life of this patent
Estimating the term…
Abstract
Products of a coprecipitation process comprising (i) substantially clear serum and (ii) homogeneous, essentially non-tacky, dustless, friable particles of predispersed rubber or plastic compounding chemical which comprise from about 80 to about 99.5 percent by weight of said chemical and from about 0.5 to about 20 percent by weight of a film-forming binder comprising a rubber or plastic polymer, wherein substantially all of the particles of the compounding chemical are at least 0.05 micron in size and no compounding chemical used is a reinforcing agent or diluent for rubber or plastic stock, are formed associatively.
Claims66
A process for improving the clarity of the serum produced during coprecipitation of a rubber or plastic compounding chemical and a binder, comprising
- (a) intimately mixing at least one finely divided rubber or plastic compounding chemical, wherein substantially all of the particles thereof are at least about 0.05 micron in size, with a film-forming binder emulsion comprising a latex of a rubber or plastic polymer in the presence of an amount of water which permits intimate mixture thereof, wherein no compounding chemical used is a reinforcing agent or diluent for rubber or plastic stock,
- (b) adding a stoichiometric excess of a coagulating agent during further intimate mixing of the chemical and the binder emulsion to cause complete coagulation thereof, and
- (c) physically separating the substantially clear serum produced upon coagulation from the homogeneous, essentially non-tacky, dustless, friable particles of predispersed chemical which comprise from about 80 to about 99.5 percent by weight of said chemical and from about 0.5 to about 20 percent by weight of said binder.
A process for improving the clarity of the serum produced during coprecipitation of a rubber or plastic compounding chemical and a binder, comprising
- (a) intimately mixing at least one finely divided rubber or plastic compounding chemical wherein substantially all of the particles thereof are at least about 0.05 micron in size, with a film-forming binder emulsion comprising a latex of a rubber or plastic polymer and an emulsion of a plasticizer for the polymer in the presence of an amount of water which permits intimate mixture thereof, wherein no compounding chemical is a reinforcing agent or diluent for rubber or plastic stock,
- (b) adding a stoichiometric excess of a coagulating agent during further intimate mixing of the chemical and the binder emulsion to cause complete coagulation thereof, and
- (c) physically separating the substantially clear serum produced upon coagulation from the homogeneous, essentially non-tacky, dustless, friable particles of predispersed chemical which comprise from about 80 to 99.5 percent by weight of said chemical and from about 0.5 to about 20 percent by weight of said binder.
A process for improving the clarity of the serum produced during preparation and coprecipitation of a rubber or plastic compounding chemical and a binder, comprising,
- (a) intimately mixing a solution of a water soluble salt containing the organic portion of the desired compounding chemical with a film-forming binder emulsion comprising a latex of a rubber or plastic polymer in the presence of an amount of water which permits intimate mixture thereof,
- (b) during further intimate mixing, adding a solution of a water soluble salt containing the metal cation desired in the compounding chemical, wherein the amount of metal cation present is in excess of that required to quantitatively react with the soluble salt containing the organic portion of the desired compounding chemical to form the desired compounding chemical and to coagulate the binder emulsion, thereby forming the desired compounding chemical and coprecipitating it with the binder substantially simultaneously, and wherein the compounding chemical prepared is not a reinforcing agent or diluent for rubber or plastic stock, and
- (c) physically separating the substantially clear serum produced upon coagulation from the homogeneous, essentially non-tacky, dustless, friable particles of predispersed chemical which comprise from about 80 to about 99.5 percent by weight of said chemical and from about 0.5 to about 20 percent by weight of said binder.
A product comprising (i) substantially clear serum and (ii) homogeneous, essentially non-tacky, dustless, friable particles of predispersed rubber or plastic compounding chemical which comprise from about 80 to about 99.5 percent by weight of said chemical and from about 0.5 to about 20 percent by weight of a binder, said product prepared in accordance with a coprecipitation process comprising,
- (a) intimately mixing at least one finely divided rubber or plastic compounding chemical wherein substantially all of the particles thereof are at least about 0.05 micron in size with a film-forming binder emulsion comprising a latex of a rubber or plastic polymer in the presence of an amount of water which permits intimate mixture thereof, wherein no compounding chemical used is a reinforcing agent or diluent for rubber or plastic stock, and
- (b) adding a stoichiometric excess of a coagulating agent during further intimate mixing of the chemical and the binder emulsion to cause complete coagulation thereof.
A product comprising (i) substantially clear serum and (ii) homogeneous, essentially non-tacky, dustless, friable particles of predispersed rubber or plastic compounding chemical which comprise from about 80 to about 99.5 percent by weight of said chemical and from about 0.5 to about 20 percent by weight of a binder, said product prepared in accordance with a coprecipitation process comprising,
- (a) intimately mixing at least one finely divided rubber or plastic compounding chemical wherein substantially all of the particles thereof are at least about 0.05 micron in size with a film-forming binder emulsion comprising a latex of rubber or plastic polymer and an emulsion of a plasticizer for the polymer in the presence of an amount of water which permits intimate mixture thereof, wherein no compounding chemical is a reinforcing agent or diluent for rubber or plastic stock, and
- (b) adding a stoichiometric excess of a coagulating agent during further intimate mixing of the chemical and the binder emulsion to cause complete coagulation thereof.
Associatively formed products of a coprecipitation process comprising (i) substantially clear serum and (ii) homogeneous, essentially non-tacky, dustless, friable particles of predispersed rubber or plastic compounding chemical which comprise from about 80 to about 99.5 percent by weight of said chemical and from about 0.5 to about 20 percent by weight of a binder comprising a rubber or plastic polymer, wherein substantially all of the particles of the compounding chemical are at least about 0.05 micron in size and no compounding chemical used is a reinforcing agent or diluent for rubber or plastic stock.
Dependencies are inferred from the claim text.