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US 4,096,316 AGranted
Method of producing magnetic material with alkaline borohydrides
AssigneeFuji Photo Film Co., Ltd.
InventorsYasuo Tamai, Masashi Aonuma
Life of this patent
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Abstract
A method of producing a magnetic material comprising reducing in a solution of a salt of a metal capable of forming a ferromagnetic material with a reducing agent comprising at least one of a borohydride and a derivative thereof, in a solution containing a hydroxide ion concentration of at least about 0.001N and not higher than about 0.6N.
Claims6
A method of producing a magnetic material for a magnetic recording medium comprising:
- (a) preparing a solution of a reducing agent selected from the group consisting of borane, borazane, borohydride, sodium borohydride, potassium borohydride, dimethylaminoborane and diethylaminoborane and a hydroxide compound selected from the group consisting of sodium hydroxide, potassium hydroxide, lithium hydroxide, ammonium hydroxide, barium hydroxide and calcium hydroxide;
- and
- (b) mixing the solution of step (a) with a solution of metal salts capable of forming a ferromagnetic material mainly comprising a ferromagnetic powder selected from the group consisting of Fe, Co, Fe-Co, Fe-Ni, Fe-Co-Ni and Co-Ni, said salt being a chloride, a sulfate, a nitrate, a formate, an acetate, a pyrophosphate, or a sulfamate;
- the concentration of reducing agent in the solution of step (a) being 0.002 to 10 mols per liter, the concentration of hydroxide ion in the solution of step (a) being 0.001 N to 0.6N, the concentration of the metal ions in said metal salt solution being 0.002 to 2 mols per liter and the ratio of borohydride to metal ion being 0.25:1 to 4:1;
- mixing step (b) being carried out at -10.degree. C to 65.degree. C and the particle size of the ferromagnetic powder product being 50 to 1000 A.
2 more elements
Dependencies are inferred from the claim text.